A kind of preparation method of composite forward osmosis membrane
A forward osmosis membrane and membrane solution technology, which is applied in the field of composite forward osmosis membrane preparation, can solve the problems of low membrane flux, and achieve the effects of increased retention capacity, high salt rejection rate, and high water flux
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Embodiment 1
[0024] An embodiment of the preparation method of the composite forward osmosis membrane described in the present invention, this embodiment uses boron nitride nanotubes, and the preparation method includes the following steps:
[0025] (1) the anionic surfactant ammonium oleate aqueous solution and the boron nitride nanotube are mixed by the ratio of adding 4 milligrams of boron nitride nanotubes per 1 milliliter of anionic surfactant with a mass concentration of 3%, and then the mixture is ultrasonically dispersed for 3 Hours, relying on the affinity of surfactant carboxylate anions to nitrogen atoms on the surface of boron nitride nanotubes to achieve surface coating, and the filtered product was dried at 80 degrees Celsius to obtain surface-modified boron nitride nanotubes.
[0026] (2) Soak the support material with a thickness of 80 microns and made of non-woven fabric in an alkaline solution with a pH of 12, and ultrasonically for more than 30 minutes at the same time, t...
Embodiment 2
[0031] An embodiment of the preparation method of the composite forward osmosis membrane described in the present invention, this embodiment uses boron nitride nanotubes, and the preparation method includes the following steps:
[0032] (1) the anionic surfactant ammonium oleate aqueous solution and the boron nitride nanotube are mixed by the ratio of adding 4 milligrams of boron nitride nanotubes per 1 milliliter of anionic surfactant with a mass concentration of 3%, and then the mixture is ultrasonically dispersed for 3 Hours, relying on the affinity of surfactant carboxylate anions to nitrogen atoms on the surface of boron nitride nanotubes to achieve surface coating, and the filtered product was dried at 80 degrees Celsius to obtain surface-modified boron nitride nanotubes.
[0033] (2) Soak the support material with a thickness of 120 microns and made of polyester mesh in an alkaline solution with a pH of 13, and ultrasonically for more than 30 minutes at the same time, th...
Embodiment 3
[0038] An embodiment of the preparation method of the composite forward osmosis membrane described in the present invention, this embodiment uses boron nitride nanotubes, and the preparation method includes the following steps:
[0039] (1) the anionic surfactant ammonium oleate aqueous solution and the boron nitride nanotube are mixed by the ratio of adding 4 milligrams of boron nitride nanotubes per 1 milliliter of anionic surfactant with a mass concentration of 3%, and then the mixture is ultrasonically dispersed for 3 Hours, relying on the affinity of surfactant carboxylate anions to nitrogen atoms on the surface of boron nitride nanotubes to achieve surface coating, and the filtered product was dried at 80 degrees Celsius to obtain surface-modified boron nitride nanotubes.
[0040] (2) Soak the support material with a thickness of 40 microns and made of non-woven fabric in an alkaline solution with a pH of 14, while ultrasonicating for more than 30 minutes, then wash it wi...
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