Control method for thermal barrier coating porosity

A control method and technology of thermal barrier coating, applied in coating, metal material coating process, air transportation, etc., can solve problems such as difficult to meet, long cycle, difficult to guarantee coating quality stability, etc., and achieve broad application prospects Effect

Active Publication Date: 2014-09-10
洛阳铭天再制造科技有限公司
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  • Summary
  • Abstract
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  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the thermal barrier coating system composed of "ceramic coating / alloy transition layer (bonding layer) / superalloy substrate" is due to the mismatch in physical, chemical and mechanical properties, as well as the complexity and complexity of the process during processing. The harsh high temperature and corrosive environment in subsequent use make it difficult for thermal barrier coatings to meet the rapidly developing national defense technology (such as the high efficiency, high stability, The demand for high-power aero-engines and heavy-duty gas turbines required by large ships)
In addition, there is still a disconnect between theory and practice in terms of the supporting research on the materials, design, and process of thermal barrier coatings and the consistency and stability requirements of coating microstructure and quality control at the production level, making thermal barrier coatings There is still a big gap between the preparation process, service life, production cost and batch stability and the international advanced level, which seriously hinders the development and application of thermal barrier coatings in the cutting-edge fields of national defense.
[0003] For plasma spraying, due to the many process parameters involved, it is difficult to ensure the stability of the coating quality during the coating deposition process, resulting in the same batch of deposited coatings often have great differences in structure
At present, engineers often rely on the adjustment of current, voltage or gas parameters to control the properties of the plasma, and conduct comparative tests in combination with sample metallographic standards and physical and chemical properties to optimize and control the coating structure. This indirect method not only requires a lot of work , long period, and often need to repeat many tests, it is difficult to meet the requirements of modern high-performance coating preparation process and structural quality control

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  • Control method for thermal barrier coating porosity
  • Control method for thermal barrier coating porosity
  • Control method for thermal barrier coating porosity

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Embodiment Construction

[0019] The method for controlling the porosity of the thermal barrier coating of the present invention comprises the following steps:

[0020] (1) use figure 1 The YSZ raw material (25-90 μm) stabilized by the yttrium oxide part shown was sprayed in seven examples (17 samples) by using the ordinary plasma spraying system APS (relatively low temperature) or the supersonic plasma spraying system SAPS (relatively high temperature) Coating, during the spraying process, the back of the substrate is cooled by compressed air, the surface temperature of the sample is controlled at 150±20°C during spraying (measured by an infrared measuring instrument), and the process parameters are adjusted. Current range: 440-808A, voltage range: 72 -147V, main gas (argon) flow range: 35-70SLPM, auxiliary gas (hydrogen) flow rate 16.6-24.3SLPM, powder feeding volume 35-40g min -1 , Spray distance 70 ~ 100mm (Table 1). The Spray Watch2i temperature measurement and speed measurement system developed...

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Abstract

The invention discloses a control method for thermal barrier coating porosity. Through adjusting plasma spraying process parameters, online measurement is performed for spraying particles of different embodiments by using Spray Watch2i to obtain particle flying speeds and particle surface temperatures under different process parameters; the particle flying speeds and surface temperatures are grouped to three areas of high-temperature and high-speed, medium-temperature and medium-speed and low-temperature and low-speed; the three areas are sprayed to obtain coating layers; and the coating porosity is obtained by performing scanning electron microscope measurement; the quantitative relation between the particle flying speeds and surface temperatures and the coating porosity is determined; and the spraying process parameters are adjusted to realize effective control of coating microstructures.

Description

technical field [0001] The invention relates to a method for controlling the microstructure of thermal barrier coatings in turbine engines and large gas turbines. Background technique [0002] Thermal barrier coatings (Thermal barrier coatings, TBCs) are a functional coating applied on the surface of a metal substrate to reduce the temperature of the substrate to ensure its normal use under high temperature conditions. This coating is currently used in gas turbine engines It is widely used on the hot end parts in the field. Its design idea is mainly to use the advantages of high melting point, low thermal conductivity and high toughness of metal materials to form a coating system (multi-layer structure) to meet the requirements of high temperature use. However, the thermal barrier coating system composed of "ceramic coating / alloy transition layer (bonding layer) / superalloy substrate" is due to the mismatch in physical, chemical and mechanical properties, as well as the comp...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C4/12C23C4/10C23C4/11C23C4/134
CPCY02T50/60
Inventor 白宇韩志海赵蕾王玉付倩倩强永明
Owner 洛阳铭天再制造科技有限公司
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