WS2 nanotile and graphene composite nanomaterial and preparation method thereof
A technology of composite nanomaterials and graphene composites, applied in nanotechnology, nanotechnology, nanotechnology for materials and surface science, etc., can solve problems such as WS2 nanowatt/graphene composite nanomaterials that have not been reported, and achieve Strong electrostatic interaction and strong hydrophobic effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0022] 1) Ultrasonically disperse 2.5 mmol of graphene oxide in 60 mL of deionized water, then add 0.8 mmol of gemini surfactant N-dodecylpropylenediamine diammonium bromide, and stir thoroughly;
[0023] 2) Then add 0.75 g (6.25 mmol) L-cysteine and 1.25 mmol ammonium thiotungstate in turn, and keep stirring to completely dissolve L-cysteine and ammonium thiotungstate, adjust with deionized water Volume up to about 80 mL;
[0024] 3) Transfer the obtained mixed solution to a 100 mL hydrothermal reaction kettle, put the reaction kettle into a constant temperature oven, and after hydrothermal reaction at 230 °C for 24 h, let it cool down to room temperature naturally, and collect the solid by centrifugation The product was washed thoroughly with deionized water and dried under vacuum at 100°C;
[0025] 4) The solid product obtained above was heat-treated at 800°C for 2 hours in a nitrogen / hydrogen mixed atmosphere to prepare WS 2 Nanowatt / graphene composite nanomaterial, ...
Embodiment 2
[0033] 1) Ultrasonically disperse 2.5 mmol of graphene oxide in 60 mL of deionized water, then add 0.8 mmol of gemini surfactant N-dodecylpropylenediamine diammonium bromide, and stir thoroughly;
[0034] 2) Then add 1.50 g (12.5 mmol) L-cysteine and 2.5 mmol ammonium thiotungstate in sequence, and keep stirring to completely dissolve L-cysteine and ammonium thiotungstate, adjust with deionized water Volume up to about 80 mL;
[0035] 3) Transfer the obtained mixture to a 100 mL hydrothermal reaction kettle, put the reaction kettle into a constant temperature oven, and after hydrothermal reaction at 220 °C for 24 h, let it cool down to room temperature naturally, and collect the solid by centrifugation The product was washed thoroughly with deionized water and dried under vacuum at 100°C;
[0036] 4) The solid product obtained above was heat-treated at 800°C for 2 hours in a nitrogen / hydrogen mixed atmosphere to prepare WS 2 Nanowatt / graphene composite nanomaterial, the ...
Embodiment 3
[0039] 1) Ultrasonically disperse 3.75 mmol of graphene oxide in 60 mL of deionized water, then add 1.2 mmol of gemini surfactant N-dodecylpropylenediamine diammonium bromide, and stir thoroughly;
[0040] 2) Then add 6.25 mmol L-cysteine and 1.25 mmol ammonium thiotungstate in sequence, and keep stirring to completely dissolve L-cysteine and ammonium thiotungstate, adjust the volume to about 80 with deionized water mL;
[0041] 3) Transfer the obtained mixed solution to a 100 mL hydrothermal reaction kettle, and add deionized water to adjust the volume to 80 mL, put the reaction kettle in a constant temperature oven, and conduct a hydrothermal reaction at 240 °C for 24 h, let It was naturally cooled to room temperature, and the solid product was collected by centrifugation, washed thoroughly with deionized water, and dried under vacuum at 100°C;
[0042] 4) The solid product obtained above was heat-treated at 800°C for 2 hours in a nitrogen / hydrogen mixed atmosphere to p...
PUM
Login to view more Abstract
Description
Claims
Application Information
Login to view more - R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap