A kind of calcium hexaaluminate foam ceramics and preparation method thereof
A technology of foam ceramics and calcium hexaaluminate, which is applied in the field of foam ceramics, can solve problems such as the influence of high temperature performance of products, long production cycle of foam method, uneven distribution of materials, etc., achieve energy saving and environmental protection technology, easy control of composition and density, and benefit The effect of environmental protection
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Embodiment 1
[0023] A calcium hexaaluminate foam ceramic and a preparation method thereof. 75-80wt% aluminum oxide fine powder and 20-25wt% calcium carbonate are used as raw materials, and 30-75wt% sugar is added to the raw materials, and the mixture is uniformly mixed to obtain a mixture. Then, the mixture is heated to 200-240° C. and stirred to obtain a dispersion system in which the raw materials are evenly dispersed in the sugar melt. Then foam and solidify the dispersion system at a constant temperature of 120-150°C for 18-26 hours, and finally burn the solidified green body at 1330-1415°C and keep it warm for 1-3 hours to obtain calcium hexaaluminate foam ceramics .
[0024] In this embodiment: alumina fine powder is α-Al 2 o 3 Fine powder; calcium carbonate is nano calcium carbonate; sugar is fructose.
[0025] The calcium hexaaluminate foam ceramics prepared in this example are tested: the bulk density is 0.33~0.38g / cm 3 ; The compressive strength is 5.91~6.47MPa.
Embodiment 2
[0027] A calcium hexaaluminate foam ceramic and a preparation method thereof. 80-85wt% aluminum oxide fine powder and 15-20wt% calcium carbonate are used as raw materials, and 75-120wt% sugar is added to the raw materials, and mixed uniformly to obtain a mixture. Then, the mixture is heated to 200-240° C. and stirred to obtain a dispersion system in which the raw materials are evenly dispersed in the sugar melt. Then the dispersion system is foamed and solidified at a constant temperature of 120-150°C for 26-34 hours, and finally the solidified body is fired at 1415-1510°C and kept for 3-5 hours to obtain calcium hexaaluminate foam ceramics .
[0028] In this embodiment: alumina fine powder is γ-Al 2 o 3 fine powder; calcium carbonate is light calcium carbonate; sugar is sucrose.
[0029] The calcium hexaaluminate foam ceramics prepared in this example are tested: the bulk density is 0.20~0.27g / cm 3 ; The compressive strength is 2.27~3.94MPa.
Embodiment 3
[0031] A calcium hexaaluminate foam ceramic and a preparation method thereof. 85-90wt% alumina fine powder and 10-15wt% calcium carbonate are used as raw materials, plus 120-165wt% sugar of the raw materials, and mixed uniformly to obtain a mixture. Then, the mixture is heated to 240-280° C. and stirred to obtain a dispersion system in which the raw materials are uniformly dispersed in the sugar melt. Then foam and solidify the dispersion system at a constant temperature of 150-180°C for 34-42 hours, and finally burn the solidified green body at 1510-1595°C and keep it warm for 5-7 hours to obtain calcium hexaaluminate foam ceramics .
[0032] In this embodiment: the alumina fine powder is industrial alumina fine powder; the calcium carbonate is nanometer calcium carbonate; and the sugar is glucose.
[0033] The calcium hexaaluminate foam ceramics prepared in this example are tested: the bulk density is 0.17~0.23g / cm 3 ; The compressive strength is 2.08~3.06MPa.
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Abstract
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