Patents
Literature
Patsnap Copilot is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Patsnap Copilot

374results about How to "Controllable shape" patented technology

Nuclear shell nanometer catalyst packaged with noble metal nanometer grains and method thereof

The invention relates to a nuclear shell nanometer catalyst packaged with noble metal nanometer grains and a method thereof, which relate to a nanometer catalyzing material. The invention provides a nuclear shell nanometer catalyst packaged with noble metal nanometer grains, which has a size of the noble metal grains less than 10nm, and higher contact level among noble metal grains and stability of the catalyst, can be reused and is adaptive to different using conditions by multi-level derivation, and also provides a preparation method thereof. The catalyst has a formula of NMP@X, NMP is nanometer grains such as Pd, AgPd or Au, and the like, and X is spherical SiO2, hollow SnO2 ball or hollow C ball. The method comprises the following steps: synthesizing noble metal nanometer grains and adorning the surface to obtain noble metal-iron oxide nanometer heterojunction; coating a silicon dioxide to obtain noble metal iron heterojunction oxide @ silicon dioxide nuclear shell nanometer material, growing porous pores on the surface, removing the silicon dioxide, and removing iron oxide on the noble metal nanometer grains so that the noble metal nanometer grains are located in a nanometer capsule of the hollow porous pores to obtain the product.
Owner:XIAMEN UNIV

Metal/grapheme nanocomposite and preparation method thereof

The invention discloses a metal/grapheme nanocomposite and a preparation method thereof. The method comprises a photo-reduction one-step method and a photocatalytic reduction one-step method. The photo-reduction one-step method comprises the steps as follows: a grapheme oxide and metal complex acid or inorganic salt and a photo-reduction agent are mixed at the room temperature or under the condition of an ice-water bath, and under the light condition, organic negative hydrogen donors reduce metal ions and the grapheme oxide, so that a product is obtained. One approach of the photocatalytic reduction one-step method comprises the steps as follows: the grapheme oxide and the metal complex acid or salt are mixed in a DMF (dimethyl formamide) water solution containing a reducing agent, a metal ligand and a photocatalyst or in a water solution, catalysis is performed through the catalyst under the light condition, and at the same time, the reducing agent reduces the metal ions and the grapheme oxide, so that a product is obtained; and the other approach of the photocatalytic reduction one-step method comprises the steps as follows: the grapheme oxide and a metal organic complex are mixed in a DMF water solution containing the reducing agent and the photocatalyst or in a water solution, then catalysis is performed through the catalyst under the light condition, and the reducing agent reduces the metal organic complex and the grapheme oxide, so that a product is obtained.
Owner:TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI

Preparation method of cadmium selenide or cadmium sulfide two-dimensional monocrystal nanosheet

The invention discloses a preparation method of a cadmium selenide or cadmium sulfide two-dimensional monocrystal nanosheet. The method comprises the steps that the CdSe or CdS two-dimensional monocrystal nanosheet is prepared through a van der Waals epitaxial growth technology, the method is characterized in that a mica sheet which is smooth in surface and free of chemical dangling bond is adopted to serve as a substrate, CdCl2 powder or Se powder or S powder serves as a source material, argon serves as carrier gas, CdCl2 stream is reacted with Se or S steam to form CdSe or CdS steam at high temperature, and the steam is deposited on the mica sheet for nucleation and epitaxially grows into the CdSe or CdS two-dimensional monocrystal nanosheet. The preparation method of the cadmium selenide or cadmium sulfide two-dimensional monocrystal nanosheet is easy to operate, low in cost and strong in controllability, the obtained CdSe or CdS has the advantages of being good in size uniformity, high in degree of crystallinity and the like, and important research value and wide application prospect in the fields of solar cells, field effect transistors, photoelectric detectors, photocatalyses and the like are achieved.
Owner:TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI

Noble metal nanocatalyst loaded on dendritic macromolecule functionalized graphene and preparation method thereof

The invention relates to a noble metal nanocatalyst loaded on a dendritic macromolecule functionalized graphene and a preparation method thereof. The nanocatalyst is composed of graphene, silane coupling agents, dendritic macromolecules and noble metal nanoclusters, wherein the dendritic macromolecules are amino-terminated polyamide-amine (PAMAM) dendritic macromolecules, and the noble metal nanoclusters comprise palladium, platinum, gold, silver, ruthenium, iridium, osmium and related alloys. Aminos are introduced onto the surfaces of exfoliated graphene by the silane coupling agents, then different generations of the dendritic macromolecules are covalently introduced, and further the nanoclusters of noble metals and the related alloys are loaded by using the above-obtained materials as templates. The loaded noble metal nanocatalyst is not easy to agglomerate or to fall off during catalytic processes, and has high catalytic activity. The loaded noble metal nanoclusters has the characteristics of tunable size and controllable shape, and the structure and composition of the noble metal alloys can be controlled accurately. The method is simple in process and short in period, and can easily realize industrial production.
Owner:HENAN UNIV OF SCI & TECH

Method for preparing titanium-based graphene composite material through 3D printing technology

The invention discloses a method for preparing a titanium-based graphene composite material through a 3D printing technology. The method includes the steps that firstly, titanium and alloy powder of the titanium are evenly mixed with graphene powder in a high-energy ball grinding manner, and titanium-based/graphene composite powder is obtained, wherein the adding amount of graphene accounts for 0.1-3 weight percent of the total mass; secondly, a stearic acid alcoholic solution is added into the evenly-mixed composite powder, ball grinding is conducted again, and composite powder obtained after the second time of ball grinding is screened and granulated, and titanium-based/graphene composite powder with the grain size ranging from 10 microns to 70 microns is obtained; and thirdly, the composite powder is packed into a powder supply box in batches, the surface of a base material is wiped through acetone, oil dirt is removed, and finally the titanium-based graphene composite material is prepared through the 3D printing technology. The 3D printing technology is used for preparing, a titanium-based graphene composite material practical part in a complex shape can be prepared according to practical needs, a prepared block material is large in size and controllable in shape, and the graphene adding amount is accurately controlled within the range of 0.1-3 weight percent; and meanwhile the preparing technology is simple, operation is convenient, and the preparing efficiency is high.
Owner:CHINA WEAPON SCI ACADEMY NINGBO BRANCH

Silicon heterojunction solar cell with electroplating electrode and manufacturing method thereof

The embodiment of the invention discloses a silicon heterojunction solar cell with an electroplating electrode and a manufacturing method thereof. The method comprises the steps that a metal seed layer is formed on the surface, where a grid needs to be manufactured, of a cell substrate; a silk-screen printing ink process is used for forming an ink grid line groove pattern on the surface of the metal seed layer; after a preset time interval, the ink grid line groove pattern is cured; the ink grid line groove pattern is used as a mask film, an electroplating process is used for depositing a composite metal layer; the ink grid line groove pattern and the part, which is not in contact with the composite metal layer, of the metal seed layer is removed. The implementation mode for forming the ink grid line groove pattern by the silk-screen printing ink process is simple and controllable, moreover, ink can be removed easily, and the manufacturing technology is simple. In the curing process, the ink can be evenly expanded and deformed, the width of an opening of the obtained ink grid line groove pattern is small, the depth-width ratio of a formed metal grid line is large, the light shading area is small, and the efficiency of the silicon heterojunction solar cell with the electroplating electrode is improved.
Owner:ENN SOLAR ENERGY

Amino end-group triazine ring tree-shaped macromolecular adsorbent and preparation method thereof

The invention relates to an amino end-group triazine ring tree-shaped macromolecular adsorbent and a preparation method thereof. An anionic dye can be removed by fading dye wastewater. A tree-shaped macromolecule is a three-dimensional hyper-branched sequential novel macromolecule, so that the size, shape structure and functional group of the molecule can be strictly controlled and designed at molecular level, a dye molecule can be wrapped by a cavity structure in the macromolecule, and the removing purpose is achieved. The preparation method provided by the invention comprises the following steps of: dissolving cyanuric chloride in acetone; adding quadrol; stirring, reacting and then adding acid-binding agent; increasing temperature and reacting; and performing suction filtration on the product and then extracting and washing, thereby obtaining the amino end-group triazine ring tree-shaped macromolecular adsorbent. Under the influence of unsaturated bonds, the adsorbent disclosed by the invention is higher in reactivity and is easily subjected to nucleophilic substitution; the reaction selectivity is excellent; the condition is controllable and the method is conducted in steps; the adsorbent has physical and chemical adsorption for the anionic dye; and the adsorbent has the characteristics of higher relative molecular mass, so that the material usage is less and the cost is low.
Owner:SHAANXI UNIV OF SCI & TECH

Method for constructing horizontal salt rock dissolving cavity reservoirs

The invention discloses a method for constructing horizontal salt rock dissolving cavity reservoirs, and belongs to categories of salt deposit water dissolving mining and salt rock dissolving cavity controlling, dissolving, constructing and utilizing. The method for constructing the horizontal salt rock dissolving cavity reservoirs has the advantages that the quick horizontal salt rock dissolving cavity reservoirs which are high in efficiency and capacity and have shapes easy to control can be constructed by means of directional drilling and cyclic retreating type single-well convection dissolving; merits of a single-well convection process and merits of double-well directional butting communication convection process are combined with one another, fresh water is injected into salt rock deposits by patterned hole jet flow sections 3 on the side walls of blind ends of center pipes, brine which is generated after salt rock is dissolved is drained out of earth surfaces from annular spaces between the center pipes and middle pipes, cavities are constructed by means of periodic sectioned retreating type dissolving, and large horizontal dissolving cavities can be constructed by means of single-well convection; the lengths of horizontal wells can reach 800-1000m, the constructed horizontal salt rock dissolving cavity reservoirs are high in capacity, and the method is a perfect method for quickly constructing the large horizontal salt rock dissolving cavity reservoirs by means of dissolving.
Owner:TAIYUAN UNIV OF TECH

Method for reducing metal and alloy hydroxide gel by hydrogen separated from electrochemistry cathode

The present invention discloses a method for reducing metal hydroxide gel and metal hydroxide-carbon gel and alloy gel and alloy hydroxide-carbon gel through electrochemical cathodic hydrogen evolution in potassium chloride aqueous solution, and directly further forming and preparing electrode materials of metal and metal-carbon and alloy and alloy-carbon. The electrode prepared by the method can obtain composition of metal: carbon or alloy: carbon with definite proportion, thereby the electrode composition is stable. The tin-carbon gel and tin-cobalt-carbon gel of the present invention is prepared by a definite proportion chemical precipitation method, and overcomes the disadvantage that the coating element content can not be accurately controlled if an electrochemical deposition method is adulterated. The experimental battery consisting of the tin-carbon anode and the lithium sheet cathode prepared with the process has 20 times circulation time and specific capacity of up to 327.4 mAh / g under 0.2 C charging and discharging current; the prepared experimental battery consisting of the tin-cobalt-carbon anode and the lithium sheet cathode has 50 times circulation time specific capacity of up to 278.5 mAh / g under 0.3 C charging and discharging current.
Owner:BEIHANG UNIV

Method for preparing gelatin microballoon embolization agent

The invention relates to a method for preparing a gelatin microballoon embolization agent, which comprises the following steps of dissolving gelatin or mixture of gelatin and medicine at 30-70 DEG C, filtering to obtain gelatin solution with 15%-60% of solid content, adding gelatin solution into oil phase liquid paraffin with mass ratio of 1%-2% of stabilizer Span 80, wherein the volume ratio of water and oil is 1/1-1/10, stirring for 15 minutes by 200-800r/min, adding cross-linking agent aldehyde compound with mass percent of 2%-50% at low temperature of 0-10 DEG C, solidifying for 1-2 hours, washing or drying the cross-linking agent to obtain the microballoon embolization agent after freeze drying or dehydration. The method has the beneficial effects that the gelatin microballoon embolization agent has certain elasticity and expansibility, the surface is smooth, the sphere is obvious, the size and the shape of the sphere is uniform, the grain size is controllable, clinical embolization effect can be improved, and side effect can be lowered, the clinical controllability is strong, antitumor drug can be added into the microballoon in manufacture process, so that double therapeutical effect of medicine treatment and embolization can be realized. The gelatin has good biocompatibility and biodegradablity, and clinical safety can be guaranteed.
Owner:杭州艾力康医药科技有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products