Tungsten disulfide composite material for motor carbon brush and preparation method thereof
A technology of tungsten disulfide and composite materials, applied in chemical instruments and methods, tungsten compounds, inorganic chemistry, etc., can solve problems affecting the life of carbon brushes and commutators, reducing the working efficiency of motors, and uneven surfaces of commutators , to improve the efficiency of carbon brush preparation, simplify the carbon brush preparation process, and achieve high work efficiency
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Embodiment 1
[0026] A ingredient
[0027] The weight of sulfur, tungsten, silicon carbide and catalyst is calculated and weighed according to the process. The ratio of the weight of sulfur to the weight of tungsten powder is 35%, the ratio of the weight of silicon carbide to the weight of tungsten powder is 1%, and the weight of catalyst rhenium (Re) The weight ratio to tungsten powder is 0.1%;
[0028] B pretreatment
[0029] (1) Make silicon carbide into 5g / L carbide suspension, tungsten powder into 20g / L suspension, add 0.5% urea of the total suspension as dispersant, control pH to 5, The two are mixed and stirred for 2 hours at a temperature of 25-35 °C and normal pressure, so that the tungsten is coated on the surface of the silicon carbide;
[0030] (2) Prepare a precursor solution with urea and absolute ethanol at a ratio of 1:3, then add catalyst and sulfur, and stir at room temperature for 20 minutes;
[0031] (3) After mixing (1) and (2) and aging for 1 hour, carry out vacuu...
Embodiment 2
[0039] A ingredient
[0040] According to the calculation and weighing of sulfur, tungsten, silicon carbide and catalyst according to the process, the ratio of the weight of sulfur to the weight of tungsten powder is 70%, the ratio of the weight of silicon carbide to the weight of tungsten powder is 10%, and the weight of catalyst rhodium (Rh) The ratio to the weight of the tungsten powder is 0.2%, and the ratio of the weight of the catalyst Pt (platinum) to the weight of the tungsten powder is 0.1%;
[0041] B pretreatment
[0042] (1) Make silicon carbide into a 7g / L carbide suspension, tungsten powder into a 25g / L suspension, add 1.5% urea of the total suspension as a dispersant, and control the pH to 4, The two were mixed and stirred for 1.5 hours at a temperature of 45°C and normal pressure, so that the tungsten was coated on the surface of the silicon carbide;
[0043] (2) Prepare a precursor solution with urea and absolute ethanol at a ratio of 1:4, then add catalys...
Embodiment 3
[0052] A ingredient
[0053] The weight of sulfur, tungsten, silicon carbide and catalyst is calculated and weighed according to the process. O The ratio of the weight of S to the weight of the tungsten powder is 0.45%, and sulfur, tungsten, silicon carbide, and Co catalysts are batched;
[0054] B pretreatment
[0055] (1) Make silicon carbide into 8g / L carbide suspension, tungsten powder into 30g / L suspension, add OP emulsifier with 1% of the total suspension as dispersant, and control the pH value. 3. The two are mixed and stirred for 0.5 to 2 hours at a temperature of 25 to 65 ° C and normal pressure, so that the tungsten is coated on the surface of the silicon carbide;
[0056] (2) Prepare precursor solution with urea and absolute ethanol at a ratio of 1:5, then add catalyst and sulfur, and stir at room temperature for 15 minutes;
[0057] (3) After mixing (1) and (2) and aging for 2 hours, carry out vacuum filtration, put the mixture after suction filtration into an a...
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