General light source response modified titanium dioxide solid acid catalyst and preparation method
A solid acid catalyst, titanium dioxide technology, applied in metal/metal oxide/metal hydroxide catalysts, physical/chemical process catalysts, chemical instruments and methods, etc., can solve the constraints of commercial application of catalysts, high energy consumption, ecological System impact and other issues, to achieve good photocatalytic degradation effect, no secondary pollution, fast degradation effect
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Embodiment 1
[0021] 1. In 50ml of water, add 1 gram of TiO 2 and 0.01g H 2 PtC1 6 , sonicated for 5 minutes to mix the reaction solution evenly, under the condition of magnetic stirring, with 100W xenon lamp as the light source, 0.5ml absolute ethanol as the sacrificial agent, and photodeposition reaction for 1 hour; then filtered, washed, dried and ground to obtain Pt / TiO 2 catalyst;
[0022] 2. Transfer the above catalyst to a polytetrafluoroethylene-lined stainless steel autoclave, add 15ml of 1mol / L sulfuric acid, and react at 100°C for 24h; wash with deionized water until no sulfate ion is detected; then Dry at 50°C for 24 hours to obtain a solid acid catalyst that responds to Pt-modified titanium dioxide with a universal light source.
Embodiment 2
[0024] 1. In 100ml of water, directly add 5 grams of TiO 2 and 0.05 g AuC1 3 , ultrasonication for 7 minutes to mix the reaction solution evenly, under the condition of magnetic stirring, with 300W xenon lamp as light source, 2ml absolute ethanol as sacrificial agent, photodeposition reaction for 2.5 hours; then through suction filtration, washing, drying and grinding, Au / TiO 2 catalyst;
[0025] 2. Transfer the above catalyst to a polytetrafluoroethylene-lined stainless steel autoclave, add 50ml of 2mol / L sulfuric acid, and react at 150°C for 12h; wash with deionized water until no sulfate ion is detected; then Dry at 105° C. for 5 hours to obtain a universal light source response Au-modified titanium dioxide solid acid catalyst.
Embodiment 3
[0027] 1. In 150ml of water, add 10 grams of TiO 2 and 0.1 g PdC1 2 , sonicated for 10 minutes to mix the reaction solution evenly, under the condition of magnetic stirring, with 200W xenon lamp as the light source, 5ml of absolute ethanol as the sacrificial agent, photodeposition reaction for 5 hours; then through suction filtration, washing, drying and grinding, Pd / TiO 2 catalyst;
[0028] 2. Transfer the above catalyst to a polytetrafluoroethylene-lined stainless steel autoclave, add 20ml of 5mol / L sulfuric acid, and react at 200°C for 6h; wash with deionized water until no sulfate ion is detected; then After drying at 75°C for 12 hours, a general-purpose light source-responsive high-efficiency titanium dioxide-modified solid acid catalyst was obtained.
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