Preparation method of open pore foamed aluminum capable of easily removing pore-forming agent

A through-hole foamed aluminum and pore-forming agent technology, which is applied in the field of metal material processing, can solve the problems affecting the tightness of the bonding between aluminum particles, the existence of holes and gaps between aluminum powder particles, and low solubility, and achieve uniform pore size , controllable porosity and simple process

Inactive Publication Date: 2015-04-08
TONGJI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In addition, since the melting point of NaCl is higher than the sintering temperature, and the solubility in water is low, the undissolved NaCl particles will corrode the matrix.
Although the strength and plasticity of the aluminum foam prepared by the sintering dissolution method are higher than those prepared by the sintering dissolution method, the process of dissolving NaCl for a long time by the sintering dissolution method will affect the compact, which will affect the bonding between aluminum particles in the next sintering process. The degree of compactness will easily cause holes and gaps between the aluminum powder particles, which will affect its strength.
Moreover, the sintering dissolution method still cannot avoid the matrix corrosion problem caused by the undissolved pore-forming agent NaCl.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Example 1: After mixing spherical ammonium bicarbonate with a particle size of 1 mm and 200 mesh aluminum powder at a volume ratio of 1:1, add anhydrous ethanol with a mass fraction of the mixed powder of 10% and mix in a mixer for 3 hours. The speed of the feeder is 80r / min, and the addition of absolute ethanol can improve the uniformity of the mixed powder; put the uniformly mixed powder in the mold for pressing, the pressing pressure is 200MPa, and the pressure is kept for 3 minutes to obtain 10×10×20mm 3 The compacted sample was then immersed in a water bath at 80°C to remove spherical ammonium bicarbonate, and then washed with deionized water and then dried in a drying oven; the dried sample was placed in a vacuum degree is 10 -2 Sinter in a Pa vacuum sintering furnace for 2h at a sintering temperature of 500°C. Through-hole foamed aluminum with a porosity of 50% is prepared by this method.

Embodiment 2

[0019] Example 2: After mixing spherical ammonium bicarbonate with a particle size of 1 mm and 200 mesh aluminum powder at a volume ratio of 1:1, add anhydrous ethanol with a mass fraction of the mixed powder of 10% and mix in a mixer for 3 hours. The speed of the feeder is 80r / min; the uniformly mixed powder is placed in the mold for pressing, the pressing pressure is 200MPa, and the pressure is kept for 3 minutes to obtain 10×10×20mm 3 The compacted sample was then soaked in a water bath at 80°C to remove spherical ammonium bicarbonate, then washed with deionized water and then dried in a drying oven; the dried sample was placed in a vacuum degree is 10 -3 Sinter in a Pa vacuum sintering furnace for 2h, and the sintering temperature is 550°C. Through-hole foamed aluminum with a porosity of 50% is prepared by this method.

Embodiment 3

[0020] Example 3: After mixing spherical ammonium bicarbonate with a particle size of 1 mm and 200 mesh aluminum powder according to a volume ratio of 3:1, add anhydrous ethanol with a mass fraction of the mixed powder of 10% and mix in a mixer for 3 hours. The speed of the feeder is 80r / min; the uniformly mixed powder is placed in the mold for pressing, the pressing pressure is 300MPa, and the pressure is maintained for 3 minutes to obtain 10×10×20mm 3 The compacted sample was then soaked in a water bath at 80°C to remove spherical ammonium bicarbonate, then washed with deionized water and then dried in a drying oven; the dried sample was placed in a vacuum degree is 10 -3 Sinter in a Pa vacuum sintering furnace for 2h, and the sintering temperature is 550°C. Through-hole foamed aluminum with a porosity of 75% is prepared by this method.

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PUM

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Abstract

The invention relates to a preparation method of an open pore foamed aluminum capable of easily removing a pore-forming agent. The preparation method of the open pore foamed aluminum comprises the following steps: firstly weighing ammonium bicarbonate and aluminite powder according to a volume ratio of (1-4) to 1, then uniformly mixing, subsequently adding absolute ethyl alcohol so as to improve the uniformity of mixed powder so as to obtain mixed powder sample, then pressing the mixed powder sample to obtain a cylindrical or strip-shaped pressed blank sample; putting the pressed blank sample in water bath for dipping to remove a spherical ammonium bicarbonate pore-forming agent, then drying the pressed blank sample in a drying oven; finally, sintering the pressed blank sample in vacuum, then cooling the pressed blank sample to the room temperature so as to obtain open pore foamed aluminum which is uniform in pore structure and controllable in porosity. The preparation method of the open pore foamed aluminum has the advantages that compared with the irregularly-shaped pore-forming agent, the foamed aluminum prepared by the spherical ammonium bicarbonate is capable of avoiding crack initiation to a great extent under the action of stress; the mechanical property of the foamed aluminum is improved; the pore-forming agent can be thoroughly removed; the corrosion of the residual pore-forming agent to an aluminum substrate can be avoided; the process period is shortened; the economic benefit is increased.

Description

technical field [0001] The invention relates to a method for preparing a through-hole foamed aluminum that is easy to remove a pore-forming agent, specifically a method for preparing a through-hole foamed aluminum with a uniform structure and excellent performance by improving the traditional sintering dissolution method by using an easier-to-remove pore-forming agent , belongs to the technical field of metal material processing. Background technique [0002] As a combination of pore phase and metal phase, porous metal foam exhibits special properties different from dense metals due to its special structure. It has light weight, large specific surface area, high specific strength, damping and vibration reduction, and good absorption. Acoustic sound insulation, energy absorption, filtering, electromagnetic shielding and other characteristics. According to the different pore structures, metal foam can be divided into two types: through-hole and closed-cell. Through pores mea...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C1/08C22C21/00
Inventor 胡正飞蔡振武张振何大海蒋凯雁莫凡
Owner TONGJI UNIV
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