Coarse whiting filler for gas-permeable membrane and preparation method of coarse whiting filler
A technology of heavy calcium carbonate and gas-permeable membranes, applied in fibrous fillers, chemical instruments and methods, and inorganic pigment treatment, etc., can solve the problem of color difference and spots of gas-permeable membranes, low strength of composite membranes, uneven dispersion of fillers in composite membranes, etc. problem, to achieve the effect of good sphericity and narrow particle size distribution
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[0032] A preparation method for a breathable membrane with heavy calcium carbonate filler, comprising the following steps:
[0033] a. The selected marble with calcium carbonate content ≥ 99% is multi-stage crushed to a diameter of 3-10mm. If it is too fine, it will easily introduce other impurities, and if it is too large, it will easily cause low grinding efficiency; then grind it in a dry state to a diameter of 40-10mm. 75μm, get marble powder;
[0034] b. In order to improve the grinding efficiency and drying efficiency, add a polymer surfactant, by weight, marble powder: water: polymer surfactant = 1: 0.2~1.5: 0.001~0.1 Mix the three; Grind the calcium carbonate powder specially for the membrane to the required index and save the grinding time, and then add any one of alumina ceramic balls, corundum balls or zirconia balls with a diameter of 1-20 mm and accounting for 30-55% of the total weight of the three , stirred for 1 to 5 hours, the stirring speed was 500 to 6000r / ...
Embodiment 1
[0050] ①Choose marble ore with calcium carbonate content ≥ 99%, crush it into small pieces with a diameter of 3mm, and put it into the ring rolling mill (the speed of the main machine is 1100r / min, the speed of the fan is 4000r / min) and get D in the dust collector. 50 50μm marble powder;
[0051] ② Take 4 tons of pure water, add 100 kg of sodium polycarboxylate (commercially available Rohm and Haas 9400) and mix evenly in a premix tank, gradually add 6 tons of marble powder obtained in step ① and keep stirring to make a premix slurry;
[0052] ③Put 800kg of zirconia balls with a diameter of 1.2mm, 1,200kg of zirconia balls with a diameter of 2.2mm, and 2,000kg of zirconia balls with a diameter of 3.8mm in the vertical mixing tank. Stirrer, stirring at a stirring speed of 1800r / min for 1.5h;
[0053] 4. The mixture after stirring is filtered through 100 meshes, and the stirring medium (reusable after cleaning) and coarse particles are filtered out to obtain about 9.3 tons of c...
Embodiment 2
[0058] ①Choose marble ore with calcium carbonate content ≥ 99%, crush it into small pieces with a diameter of 8mm and put it into a ball mill (the speed of the main machine is 600r / min, the speed of the fan is 2000r / min) and get D in the dust collector 50 40μm marble powder;
[0059] ② Take 2.5 tons of pure water, add 120 kg of sodium polyacrylate (commercially available molecular weight greater than 10,000) and mix evenly in a premix tank, gradually add 5.5 tons of powder obtained in step ① and keep stirring to make a premix slurry;
[0060] ③Put 1200kg of zirconia balls with a diameter of 2mm, 800kg of zirconia balls with a diameter of 4mm, and 700kg of zirconia balls with a diameter of 6mm in the vertical mixing tank, gradually pump the premixed slurry prepared in step ② and open it from slow to fast at the same time Stirrer, stirring at a stirring speed of 1200r / min for 2h;
[0061] 4. the mixture after the stirring and grinding is filtered through a gap of 80 meshes, and...
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