Differential-shrinkage cotton-like composite filament and preparation method thereof
A composite yarn and differential shrinkage technology, which is applied in the field of fiber manufacturing, can solve the problems of increased air content in PET differential shrinkage mixed fiber composite yarn fabrics, etc.
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[0088] Example 1
[0089] A preparation method of cotton-like different shrinkage composite yarn includes the following steps:
[0090] (1) Preparation of amino fatty acid glycol ester:
[0091] 1) Add dodecane dicarboxylic acid and methanol into the reactor in a molar ratio of 1:1.5, heated to 80°C under the catalysis of concentrated sulfuric acid, reflux esterification, cooling, separation and purification to obtain dodecane dicarboxylic acid Monomethyl acid; the concentrated sulfuric acid refers to sulfuric acid with a mass concentration of 70%, and the added amount of concentrated sulfuric acid is 3wt% of dodecane dicarboxylic acid;
[0092] 2) The monomethyl dodecane dicarboxylate, lead tetraacetate and lithium bromide are dissolved in benzene (molar ratio 1:1:1), wherein the concentration of monomethyl dodecane dicarboxylate is 0.05 mol / L , In a nitrogen atmosphere, react at 80°C and reflux. When no more gas is generated, add a certain amount of dilute sulfuric acid to react fo...
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[0137] Example 2
[0138] A preparation method of cotton-like different shrinkage composite yarn includes the following steps:
[0139] (1) Preparation of amino fatty acid glycol ester:
[0140] 1) Put penictodecane dicarboxylic acid and methanol into the reactor in a molar ratio of 1:1.5, catalyzed by concentrated sulfuric acid, heated to 110°C, refluxed for esterification, cooled, and separated and purified to obtain penicodecane Monomethyl dicarboxylate; the concentrated sulfuric acid refers to sulfuric acid with a mass concentration of 70%, and the added amount of concentrated sulfuric acid is 3wt% of Pentadodecane dicarboxylic acid;
[0141] 2) Dissolve the said pentadodecane dicarboxylic acid monomethyl ester, lead tetraacetate and lithium bromide in benzene (molar ratio 1:1:1), wherein the concentration of pentadodecane dicarboxylic acid monomethyl ester is 0.07 mol / L, under nitrogen atmosphere, react at 85℃, reflux, when no more gas is generated, add a certain amount of dilu...
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[0185] Example 3
[0186] A preparation method of cotton-like different shrinkage composite yarn includes the following steps:
[0187] (1) Preparation of amino fatty acid glycol ester:
[0188] 1) Add pentadecane dicarboxylic acid and methanol to the reactor in a molar ratio of 1:1.5, catalyze by concentrated sulfuric acid, heat to 85°C, reflux and esterify, cool, separate and purify to obtain pentadecane dicarboxylic acid Monomethyl acid; the concentrated sulfuric acid refers to sulfuric acid with a mass concentration of 70%, and the added amount of concentrated sulfuric acid is 3wt% of pentadecane dicarboxylic acid;
[0189] 2) Dissolve the monomethyl pentadecane dicarboxylate, lead tetraacetate and lithium bromide in benzene (molar ratio 1:1:1), wherein the concentration of monomethyl pentadecane dicarboxylate is 0.08 mol / L , Under a nitrogen atmosphere, react at 90°C and reflux. When no gas is generated, add a certain amount of dilute sulfuric acid to react for 2.5 hours, then w...
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