A fully permeable mutant grouting material
A mutation-type, epoxy grouting technology, applied in the field of chemical grouting materials, can solve the problems of poor controllability, slowness, and impossibility of full penetration of fine cracks, and achieve the effect of stable reaction, good toughness, and increased hydrophilicity
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Embodiment 1
[0064] Preparation of phenalkamine
[0065] After mixing cardanol and low-molecular polyetheramine, conduct heat treatment, stir while heating, when the temperature rises to 80-85°C, gradually add formaldehyde dropwise to cardanol and low-molecular polyetheramine for 3-4 hours The reflux reaction, vacuum dehydration, distillation until the liquid phase temperature is 120 ° C to stop, wherein the ratio of cardanol, low molecular weight polyetheramine and formaldehyde is 1:1:1, to obtain the phenalkamine compound.
Embodiment 2
[0067] Preparation of phenalkamine
[0068] After mixing cardanol and low-molecular polyetheramine, conduct heat treatment, stir while heating, when the temperature rises to 80-85°C, gradually add formaldehyde dropwise to cardanol and low-molecular polyetheramine for 3-4 hours Reflux reaction, vacuum dehydration, distillation to stop at liquid phase temperature of 120°C, wherein the ratio of cardanol, low-molecular polyetheramine and formaldehyde is 1:1:2, and the phenalkamine compound is obtained.
Embodiment 3
[0070] Preparation of phenalkamine
[0071] After mixing cardanol and low-molecular polyetheramine, conduct heat treatment, stir while heating, when the temperature rises to 80-85°C, gradually add formaldehyde dropwise to cardanol and low-molecular polyetheramine for 3-4 hours The reflux reaction, vacuum dehydration, distillation to a liquid phase temperature of 120 ° C to stop, wherein the ratio of cardanol, low molecular weight polyetheramine and formaldehyde is 1:2:2, to obtain phenalkamine compound.
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