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Ultrafine semi-dull high-strength low-elongation viscose fiber and preparation method thereof

A viscose fiber, high-strength and low-elongation technology, which is applied in the field of ultra-fine semi-matte high-strength and low-elongation viscose fiber and its preparation, can solve the problem that the market share of viscose fiber is reduced, and the development of new downstream textiles cannot be met to a greater extent. and industrial upgrading, etc., to achieve the effect of high product strength, good color fastness and good air permeability of finished products

Active Publication Date: 2015-08-19
YIBIN GRACE GROUP CO LTD +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] Only the above-mentioned published patent documents can know that in order to produce differentiated and functional viscose fibers, the prior art is realized by changing the production process, which involves raw materials, viscose molding and its process parameters Compared with ordinary viscose fiber, the obtained viscose fiber has been properly optimized in terms of fineness and strength, but for the increasingly fierce market competition, the differentiated viscose fiber does not meet the downstream needs to a greater extent. The development of new textiles and industrial upgrading, especially the development of fiber raw materials such as tencel, modal, and cupro fibers, which are also regenerated from natural cellulose materials, have reduced the market share of viscose fibers.

Method used

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  • Ultrafine semi-dull high-strength low-elongation viscose fiber and preparation method thereof
  • Ultrafine semi-dull high-strength low-elongation viscose fiber and preparation method thereof
  • Ultrafine semi-dull high-strength low-elongation viscose fiber and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0063] The pulp raw material is sequentially soaked, ground, crushed, kneaded, depolymerized, yellowed, dissolved, filtered, defoamed, matured, matting agent is added, spinning and drawing, refining and drying to obtain semi-dull viscose. Glue fiber, the semi-dull viscose fiber of the present embodiment has following performance index system:

[0064] The fineness is 1.67 dtex, the dry breaking strength is 3.12 cN / dtex, the wet breaking strength is 1.65cN / dtex,

[0065] The strength required to produce 5% elongation in wet state is 0.55cN / dtex,

[0066] Dry elongation at break is 19.0%, wet elongation at break is 21.0%,

[0067] The crystallinity is 40%, the radial water swelling degree is 22%, and the content of matting agent is 0.10%.

[0068] The linear density deviation rate is -11.0%, the residual sulfur is 8.0mg / 100g,

[0069] The length deviation rate is -11.0%, the ultra-long fiber rate is 0.48%, and the whiteness is 84.1%.

[0070] The double-length fiber is 4.0mg...

Embodiment 2

[0072] The difference between the superfine type semi-dull high-strength low-elongation viscose fiber of the present embodiment and embodiment 1 is: the present embodiment has the following indicators:

[0073] Denier is 1.52 dtex, dry breaking strength is 3.15 cN / dtex, wet breaking strength is 1.67cN / dtex,

[0074] The strength required to produce 5% elongation in wet state is 0.54cN / dtex,

[0075] The dry elongation at break is 18.9%, and the wet elongation at break is 20.8%.

[0076] The crystallinity is 40%, the radial water swelling degree is 22.5%, and the matting agent content is 0.75%.

[0077] The whiteness is 84.6%, the linear density deviation rate is -10.0%, the residual sulfur is 8.0mg / 100g,

[0078] The length deviation rate is +10.0%, and the ultra-long fiber rate is 0.5%,

[0079] The double-length fiber is 4.0mg / 100g, and the defect is 4.0mg / 100g.

Embodiment 3

[0081] In order to better implement the present invention, this embodiment further provides the specific preparation method of the superfine semi-dull high-strength low-elongation viscose fiber of the present invention, and measures the performance index.

[0082] A method for preparing semi-dull viscose fiber: the pulp raw material is soaked and pressed to remove the lye to obtain alkali cellulose; Cellulose; the obtained methyl cellulose is yellowed to obtain cellulose sulfonate; the obtained cellulose sulfonate is dissolved in a solvent, then filtered, matured, defoamed, and the spinning solution is obtained; the obtained spinning After the silk liquid is added with a matting agent, it is sent to a spinning machine for spinning and drawing to obtain a tow, and the tow is refined and dried to obtain the viscose fiber of the present invention. Samples were taken, and each index was measured according to the above-mentioned measurement standards.

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Abstract

The invention provides an ultrafine semi-dull high-strength low-elongation viscose fiber and a preparation method thereof. The viscose fiber is obtained by sequentially performing soaking, grinding, squeezing crushing, kneading, polymerization reduction, yellowing, dissolving, filtering, defoaming, curing, spinning drawing and after-treatment on a pulp raw material, and has the following indexes that the fineness is 0.8-1.11dtex, the dry fracture strength is more than or equal to 3.10cN / dtex, the wet fracture strength is more than or equal to 1.60cN / dtex, the strength needed for generating 5% of the elongation in a wet state is more than or equal to 0.55cN / dtex, and the dry elongation at break is 11.0-19.0%. The ultrafine high-strength low-elongation viscose fiber is a novel fiber variety realized by virtue of technical innovation, and has an index system which is different from that of ordinary viscose fibers and Modal fibers, and a product of the fiber shows the fiber characteristics of high strength and low elongation of the Modal fibers and also shows skin affinity stronger than that of cotton fibers, so that the ultrafine semi-dull high-strength low-elongation viscose fiber can effectively replace the existing differentiation viscose fiber, and while the processability of the downstream process of the viscose fiber is improved, the development and the industrial upgrading of downstream novel textiles are promoted.

Description

technical field [0001] The invention relates to the technical field of viscose fiber, in particular to an ultrafine semi-dull high-strength low-elongation viscose fiber and a preparation method thereof. Background technique [0002] Textile fiber raw materials are mainly divided into natural fiber raw materials represented by cotton and hemp, petroleum-based fiber raw materials represented by polyester and acrylic fibers, and tencel, cupro ammonia fiber, Viscose fiber and other bio-based fiber raw materials. Cotton fiber is well-known for its comfort, softness, breathability, and close-fitting qualities. It accounts for about 36% of the total textile fiber market. The nutritional content of cotton, and the reduction of cotton planting soil area in countries all over the world to ensure the food supply of the global population have limited the cultivation of cotton, and the shortage of cotton fiber raw materials cannot meet the growing needs of people's living standards. V...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F2/12D01F1/10D01D5/06
Inventor 冯涛邓传东李蓉玲贺敏胡远成陈明付陈晓芳
Owner YIBIN GRACE GROUP CO LTD
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