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A kind of botanical pesticide and preparation method thereof

A technology of botanical pesticides, Daphne chamaejasme, which is applied in botany equipment and methods, plant protection, horticultural methods, etc., can solve the problems of large investment in research and development of new pesticide varieties, complex components of botanical pesticides, and obstacles to research work, etc. , to achieve the effect of high selectivity, not easy to produce resistance, and easy to degrade

Active Publication Date: 2017-06-23
黑龙江省农业科学院经济作物研究所
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] However, due to the large investment in the research and development of new pesticide varieties, the long cycle of putting them on the market, and the research on the mixing of botanical pesticides is still in its infancy, and the composition of botanical pesticides is relatively complex, so the research work is brought many obstacles

Method used

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  • A kind of botanical pesticide and preparation method thereof
  • A kind of botanical pesticide and preparation method thereof
  • A kind of botanical pesticide and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0048] Embodiment 1, preparation botanical pesticide

[0049] Prepare botanical pesticides according to the following steps:

[0050] (1) Extraction: Dry the rhizome and Zanthoxylum bungeanum fruit in an oven at 60°C respectively, pulverize them into powder with a pulverizer, and pass through a 40-mesh sieve;

[0051] Add 15 times the volume fraction of 60% ethanol aqueous solution (that is, add 15mL of 60% ethanol aqueous solution to 1g of Daphne chamaejasma powder) into the Stylus chamaejasma powder, and ultrasonically (power 100Hz) leaching three times at 25°C, 24 hours each time, combine the extracts, filter, and extract the Deruixiang chamaejasma;

[0052] Add 10 times the volume fraction of 60% ethanol aqueous solution to Zanthoxylum bungeanum powder (that is, add 10mL of 60% ethanol aqueous solution to 1g Zanthoxylum bungeanum powder), leaching three times with ultrasonic (power 100Hz) at 25°C, each time for 24h, and combine The extract is filtered to obtain the Zanth...

Embodiment 2

[0056] Embodiment 2, preparation botanical pesticide

[0057] Prepare botanical pesticides according to the following steps:

[0058] (1) Extraction: Dry the rhizome and Zanthoxylum bungeanum fruit in an oven at 60°C respectively, pulverize them into powder with a pulverizer, and pass through a 40-mesh sieve;

[0059] Add 10 times the volume fraction of 80% ethanol aqueous solution (i.e., add 10 mL of 80% ethanol aqueous solution to 1 g of Daphne chamaejasma powder) into the Stylus chamaejasma powder, and ultrasonically (power 100 Hz) leaching three times at 25 ° C, 12 hours each time, combine the extracts, filter, and extract the Deruixiang chamaejasma;

[0060] Add 5 times the volume fraction of 80% ethanol aqueous solution to Zanthoxylum bungeanum powder (that is, add 5 mL of 80% ethanol aqueous solution to 1 g Zanthoxylum bungeanum powder), leaching three times with ultrasonic (power 100 Hz) at 25 ° C, each time for 12 hours, and combine The extract is filtered to obtain...

Embodiment 3

[0064] Embodiment 3, preparation botanical pesticide

[0065] Prepare botanical pesticides according to the following steps:

[0066] (1) Extraction: Dry the rhizome and Zanthoxylum bungeanum fruit in an oven at 60°C respectively, pulverize them into powder with a pulverizer, and pass through a 40-mesh sieve;

[0067] Add 10 times the volume fraction of 70% ethanol aqueous solution (that is, add 10mL of 70% ethanol aqueous solution to 1g of Daphne chamaejasma powder) into the Stolphin chamaejasma powder, and ultrasonically (power 100Hz) leaching three times at 25°C, 24 hours each time, combine the extracts, filter, and extract the Deruixiang chamaejasma;

[0068] Add 5 times the volume fraction of 70% ethanol aqueous solution to Zanthoxylum bungeanum powder (that is, add 5 mL of 70% ethanol aqueous solution to 1 g Zanthoxylum bungeanum powder), leaching three times with ultrasonic (power 100 Hz) at 25 ° C, each time for 24 hours, and combine The extract is filtered to obtain...

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Abstract

The invention discloses a botanical pesticide and a preparation method thereof. The preparation method of the botanical pesticide comprises steps as follows: (1), Chinese stellera roots are extracted in an organic solvent I and filtered, a Chinese stellera root extracting solution is obtained, Chinese red pepper is extracted in the organic solvent I and filtered, and a Chinese red pepper extracting solution is obtained; (2), the Chinese stellera root extracting solution and the Chinese red pepper extracting solution obtained in the step (1) are evaporated respectively, and Chinese stellera root extract and Chinese red pepper extract are obtained; (3), the Chinese stellera root extract obtained in the step (2) is extracted with an organic solvent II, Chinese stellera root extract liquor is obtained, the Chinese red pepper extract obtained in the step (2) is extracted with an organic solvent III, and Chinese red pepper extract liquor is obtained; (4) the Chinese stellera root extract liquor and the Chinese red pepper extract liquor which are obtained in the step (3) are mixed, cnidium lactone is added, the mixture is stirred, and the botanical pesticide is obtained. The botanical pesticide is efficient, low-toxicity, broad-spectrum and applicable to pests such as plutella xylostella, lipaphis erysimi, sitophilus zeamais motschulsky, rhizopertha dominica fabricius, tribolium ferrugineum fabricius and the like, on crops and can also effectively control diseases such as powdery mildew, downy mildew, blight and the like.

Description

technical field [0001] The invention relates to a pesticide and a preparation method thereof, in particular to a botanical pesticide and a preparation method thereof. Background technique [0002] In agricultural production, pesticides are an indispensable means of production. Most of the pesticides currently on the market are chemical pesticides. The large and unreasonable use of chemical pesticides has caused a series of problems such as toxic substance residues and drug resistance, which not only seriously threatens the ecological environment. environment, and endanger human safety and agricultural production, has gradually become an important factor restricting the development of my country's agriculture. [0003] Compared with chemical pesticides, botanical pesticides have the advantages of high selectivity, low toxicity, easy degradation, and less resistance. In addition to active ingredients that can significantly prevent and control harmful organisms such as pests and...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A01N65/36A01P7/04A01P1/00A01P3/00A01G7/06A01G13/00A01N43/16
CPCY02A50/30
Inventor 赵茜吴建忠徐丽珍张丽艳陈洪生
Owner 黑龙江省农业科学院经济作物研究所