Method for preparing nanometer ZnS/cellulose complex film with photocatalytic activity
A photocatalytic activity, cellulose technology, applied in chemical instruments and methods, organic compound/hydride/coordination complex catalysts, chemical/physical processes, etc., can solve problems such as easy agglomeration and poor stability of inorganic nano-ZnS particles , to achieve the effect of improving catalytic activity, simple equipment, low consumption of chemical raw materials and low energy consumption
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Embodiment 1
[0033] 1. Preparation of Cellulose Membrane
[0034] One of the 2g cotton pulp cellulose, wood pulp cellulose or straw pulp cellulose after pulverization is added to the NMMO solvent and 0.02g ascorbic acid (mass approx. 1% of the element weight) in a beaker, prepare a casting solution with a cellulose content of about 6%, and stir evenly; after swelling for 2 hours, put it in a vacuum drying oven at 110°C to dissolve completely, and wait until the solution is amber and uniform When the solution is transparent, place it at 80°C for vacuum defoaming for 4 hours, and scrape the film; then, treat it with a coagulation bath (about 25°C deionized water) and a water bath (about 25°C deionized water) to obtain wet pure cotton pulp fibers plain film.
[0035] 2. Preparation of nano-ZnS / cellulose composite membrane material with photocatalytic activity
[0036] Cut the above wet film into a film with a size of 10cm×15cm, soak it in 0.1M zinc sulfate precursor solution, react for 5h, ...
Embodiment 2
[0038] 1. Preparation of Cellulose Membrane
[0039] The preparation of the cellulose film was the same as in Example 1.
[0040] 2. Preparation of nano-ZnS / cellulose composite membrane material with photocatalytic activity
[0041] Cut the above wet film into a film with a size of 10cm×15cm, soak it in 0.1M zinc sulfate precursor solution, react for 5h, take it out and rinse it with deionized water; then put it into 0.1M sodium sulfide After reacting for 5 hours in the precursor solution, take it out and rinse it with deionized water. The above process is a cycle, and then the second cycle of impregnation experiment is carried out. After the impregnation is completed, the sample film is naturally dried at room temperature to obtain a nano-ZnS / cellulose composite membrane material with photocatalytic activity that is impregnated twice.
Embodiment 3
[0043] 1. Preparation of Cellulose Membrane
[0044] The preparation method of the cellulose film is the same as that of Example 1.
[0045] 2. Preparation of nano-ZnS / cellulose composite membrane material with photocatalytic activity
[0046]Cut the above wet film into a film with a size of 10cm×15cm, soak it in 0.1M zinc sulfate precursor solution, react for 5h, take it out and rinse it with deionized water; then put it into 0.1M sodium sulfide After reacting for 5 hours in the precursor solution, take it out and rinse it with deionized water. The above process is a cycle, and then repeat the impregnation experiment twice. After the impregnation is completed, the sample film is naturally dried at room temperature to obtain a nano-ZnS / cellulose composite membrane material with photocatalytic activity that has been impregnated three times.
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