Tobacco extractive particle and preparation method thereof
A technology of tobacco extract and particles, applied in the field of tobacco, can solve the problems of nicotine release speed, release volume reduction, taste and quality decline, loss of slow release function, etc., to improve release uniformity, dense content, ensure Mouthfeel and Flavor Effects
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Embodiment 1
[0054] (1) Preparation of tobacco extract
[0055] S11. Take flue-cured tobacco with an absolute dry mass of 100g, add 1400g of water to soak at 60°C for 25min, cool to about 20°C, extract ultrasonically for 60min at 25±2°C, the power of ultrasonic wave is 300W, and then vacuum suction and filter , to obtain filter residue a and filtrate a;
[0056] S12. After adding ethanol 7 times the absolute dry mass of the filter residue a to the filter residue a of S11, ultrasonically extract for 30 minutes at 25±2°C, the power of the ultrasonic wave is 300W, and then vacuum suction and filter to obtain the filter residue b and filtrate b ;
[0057] S13. Mix filtrate a and filtrate b, and concentrate in vacuum at 25°C to a solid content of 15%, to obtain the tobacco extract.
[0058] (2) Preparation of tobacco extract particles
[0059] S21. Mix the tobacco extract prepared in (1) with starch evenly, and add an appropriate amount of water to make a soft material;
[0060] S22. Put th...
Embodiment 2~3 and comparative example 1~3
[0071] The preparation steps of Examples 2-3 of the present invention and Comparative Examples 1-3 are similar to Example 1, except that they are as shown in the following table:
[0072] Process parameters Example 2 Example 3 Comparative example 1 Comparative example 2 Comparative example 3 S11 Amount of water added, g 1300 1500 1200 1600 1500 S12 The amount of ethanol added, times 6 8 5 9 8 S11 / S12 ultrasonic temperature, ℃ 20±2 25±2 20±2 35±2 25±2 S11 / S12 ultrasonic power, W 250 350 300 250 300 S21 Excipients dextrin microcrystalline cellulose dextrin microcrystalline cellulose microcrystalline cellulose S22 extrusion speed, r / min 80 150 70 160 150 S22 Rolling speed, r / min 250 350 240 360 350 S23 / S24 / S25 fluidization temperature, ℃ 40 45 35 50 45 S23 / S24 / S25 spray flow ml / min 0.6 0.9 0.5 1.0 0.9 S23 / S24 / S25 atomizing gas pressure, Mpa 0.2 0.4 0.1 05...
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