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A kind of preparation method of high-precision ceramic ferrule

A ceramic ferrule, high-precision technology, applied in the field of ceramic electronic components, can solve the problems of easy deformation of the ferrule, low precision, easy cracks, etc., and achieve the effects of excellent thermal stress performance, high precision, and not easy to crack

Active Publication Date: 2018-02-27
NINGBO BRIGHT PHOTOELECTRIC TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The ceramic ferrule in the prior art is easily deformed, prone to cracks, and has low precision

Method used

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  • A kind of preparation method of high-precision ceramic ferrule
  • A kind of preparation method of high-precision ceramic ferrule
  • A kind of preparation method of high-precision ceramic ferrule

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preparation example Construction

[0035] The embodiment of the present invention discloses a method for preparing a high-precision ceramic ferrule, which includes the following steps:

[0036] Step a) mixing silicon oxide, scandium oxide, molybdenum oxide, holmium oxide, zinc oxide and zirconia, adding oleic acid after pre-calcination, mixing by ball milling, and obtaining partially stabilized zirconia powder after sieving;

[0037] Step b) Add the partially stabilized zirconia powder and HDPE (high-density polyethylene) into the internal mixer, add polyethylene glycol monomethyl ether and polyethylene wax after mixing, and add ethylene-vinyl acetate copolymer after stirring , TPEE (thermoplastic polyester elastomer), PTT (polytrimethylene terephthalate) and polyoxymethylene, stir, heat up to 140-150°C, then add dioctyl phthalate, stir and heat up to 160-180°C ℃, cooling after banburying to obtain a gelatinous substance;

[0038] Step c) compressing the gelatinous substance into tablets, pulverizing it, and o...

Embodiment 1

[0085] Step 1, preparing partially stabilized zirconia powder,

[0086] Mix 1 part by weight of silicon oxide, 2 parts by weight of scandium oxide, 1 part by weight of molybdenum oxide, 1 part by weight of holmium oxide, 1 part by weight of zinc oxide and 94 parts by weight of zirconia Pre-sintering was carried out for 2 hours, and then 4 parts by weight of oleic acid was added for ball milling, mixing and sieving to obtain partially stabilized zirconia powder.

[0087] Step 2. Mixing of ceramic powder and organic binder

[0088] Mix the partially stabilized zirconia powder prepared above with organic carriers such as binders, surface active agents and plasticizers in a certain proportion. The raw materials used in this step include in parts by weight:

[0089]

[0090] First raise the temperature of the internal mixer to 105°C, then add the corresponding parts by weight of the partially stabilized zirconia powder substrate and HDPE prepared in step 1 to the above internal...

Embodiment 2

[0110] Step 1, preparing partially stabilized zirconia powder,

[0111] Mix 1 part by weight of silicon oxide, 2 parts by weight of scandium oxide, 1 part by weight of molybdenum oxide, 1 part by weight of holmium oxide, 1 part by weight of zinc oxide and 94 parts by weight of zirconia Pre-sintering was carried out for 2 hours, and then 4 parts by weight of oleic acid was added for ball milling, mixing and sieving to obtain partially stabilized zirconia powder.

[0112] Step 2. Mixing of ceramic powder and organic binder

[0113] Mix the partially stabilized zirconia powder prepared above with organic carriers such as binders, surface active agents and plasticizers in a certain proportion. The raw materials used in this step include in parts by weight:

[0114]

[0115] First raise the temperature of the internal mixer to 105°C, then add the corresponding parts by weight of the partially stabilized zirconia powder substrate and HDPE prepared in step 1 to the above internal...

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Abstract

The invention provides a preparation method of a high-precision ceramic ferrule and a preparation method of partially stabilized zirconium oxide powder for the high-precision ceramic ferrule. The preparation methods provided by the invention have the following advantages: firstly, silicon oxide, molybdenum oxide, zinc oxide, scandium oxide and holmium oxide are adopted, so that the thermal stress property of partially stabilized zirconium ceramic is high, the thermo-mechanical property of zirconium oxide is improved, and the ferrule material can be higher in strength, high in thermal shock resistance, low in deformation possibility and free from cracking; secondly, through an ethylene-vinyl acetate copolymer, TPEE, PTT, HDPE, polyformaldehyde and the like are polymerized in an interpenetrated manner to form an interpenetrated network structure, so that the obtained ceramic ferrule is low in deformation possibility and relatively high in precision; thirdly, an adopted organic binding agent has high liquidity, so that the ceramic ferrule is high in homogeneity and free from cracking; finally, due to the sequence of adding the organic binding agent during mixed refining, the feeding rheological property can be relatively high, a blank material can be easier to degrease, and then the prepared ceramic ferrule can be prevented from cracking.

Description

technical field [0001] The invention relates to the technical field of ceramic electronic components, in particular to a method for preparing a high-precision ceramic ferrule. Background technique [0002] In the field of optical fiber communication technology, optical fiber connectors can be used to transmit optical signals, and their core and basic components are ferrules, which play the role of media for connection, conversion, and data transmission. They are the most basic and important components of a series of optical communication products. Passive components. [0003] The most widely used ceramic material at present is zirconia ceramic ferrule, which is prepared by injection molding of zirconia powder. The injection molding process technology originated from the field of plastic molding and was later extended to the molding of ceramics. The basic process includes pretreatment of powder, heating and mixing of powder and binder to form feed, and after the feed is cool...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/48C04B35/634
Inventor 曹波
Owner NINGBO BRIGHT PHOTOELECTRIC TECH
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