Preparation method of thermal conducting and insulating material of LED substrate
A technology of thermally conductive insulating material and LED substrate, applied in the field of material chemistry, can solve the problems of poor physical properties and thermal conductivity of thermally conductive resin materials, poor bending and kink resistance, and poor compression and shock resistance. The branch copolymerization reaction is sufficient, the rate is fast, and the effect of increasing stiffness
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Embodiment 1
[0032] This embodiment provides a thermally conductive insulating material for a high-power LED substrate, and the thermally conductive insulating material for a high-power LED substrate is prepared through the following steps:
[0033] (1) In parts by mass, add 30 parts of silicon oxide powder with an average particle size of 10nm to 3 parts of graft modifier maleic anhydride, then add 0.1 part of dispersant to polyacrylamide, and stir for 10 to 15 minutes. Then use ultrasonic dispersion for 20-30 minutes to disperse the nano-silica powder in the mixed solvent of maleic anhydride and polyacrylamide to form an emulsion-like dispersion;
[0034] (2) the emulsion-like dispersion prepared in the above-mentioned steps (1) is added to ultrasonic spray drying equipment and spray-dried to prepare a powdery composite material comprising nano-silicon oxide;
[0035] (3) Add the powdery composite material prepared in the above step (2) together with 7 parts of polypropylene resin powder...
Embodiment 2
[0042] This embodiment also provides a thermally conductive insulating material for a high-power LED substrate. The thermally conductive insulating material for a high-power LED substrate is prepared through the following steps:
[0043] (1) Add 80 parts of alumina powder with an average particle size of 30nm in 20 parts of graft modifier oleic acid, then add 10 parts of dispersant as sodium lauryl sulfate, and stir for 10~ 15 minutes, and then use ultrasonic dispersion for 20-30 minutes to disperse the nano-alumina powder in a mixed solvent of oleic acid and sodium lauryl sulfate to form an emulsion-like dispersion;
[0044] (2) the emulsion-like dispersion prepared in the above-mentioned steps (1) is added to ultrasonic spray drying equipment and spray-dried to prepare a powdery composite material comprising nano-silicon oxide;
[0045] (3) The powdered composite material prepared in the above-mentioned step (2) and 40 parts of polyethylene resin powder are added to the twin...
Embodiment 3
[0052] This embodiment also provides a thermally conductive insulating material for a high-power LED substrate. The thermally conductive insulating material for a high-power LED substrate is prepared through the following steps:
[0053] (1) In parts by mass, add 30 parts of magnesium oxide powder with an average particle size of 50nm to 20 parts of graft modifier acrylic acid, then add 10 parts of dispersant as fatty acid polyethylene glycol ester, and stir for 10 to 15 minutes , and then use ultrasonic dispersion for 20 to 30 minutes to disperse the nano magnesium oxide powder in a mixed solvent of acrylic acid and fatty acid polyethylene glycol ester to form an emulsion-like dispersion;
[0054] (2) join the emulsion-like dispersion made in above-mentioned steps (1) to ultrasonic spray drying equipment and carry out spray-drying and prepare powdery composite material comprising nano magnesium oxide;
[0055] (3) The powdered composite material prepared in the above step (2) i...
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