Preparation method of a portable clean energy micro-storage device
A technology of clean energy and storage equipment, applied in the field of preparation of portable clean energy micro storage equipment, can solve the problems of excellent stability and rate performance, low price, etc., and achieve the effect of easy portability, easy operation, and easy industrialization
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specific Embodiment approach 1
[0022] Specific embodiment 1: This embodiment is a method for preparing a portable clean energy micro storage device through the following steps:
[0023] 1. Cleaning of the current collector: Place the current collector in water for ultrasonic cleaning for 5 min to 120 min, then place it in ethanol for ultrasonic cleaning for 5 min to 300 min, and finally place it in a dilute hydrochloric acid solution with a concentration of 0.01 mol / L to 6 mol / L. 5min~200min, get clean current collector;
[0024] 2. Mix the cobalt nitrate solution with the concentration of 0.0001mol / L~1mol / L and the urea solution with the concentration of 0.0001mol / L~1mol / L and stir for 5min~720min to obtain the mixed solution A. The clean solution obtained in step 1 The current collector is immersed in the mixed solution A, and then transferred to the reactor. After heating for 0.5h to 72h at a temperature of 90°C to 200°C, the product is taken out of the reactor, and the product is washed with water 3 to 5 tim...
specific Embodiment approach 2
[0030] Specific embodiment two: this embodiment is different from specific embodiment one in that in step one, it is ultrasonically cleaned in a dilute hydrochloric acid solution with a concentration of 0.08 mol / L for 40 minutes. Others are the same as the first embodiment.
specific Embodiment approach 3
[0031] Specific embodiment three: This embodiment is different from specific embodiment one or two in that in step two, heating is performed at a temperature of 100° C. for 1 hour. Others are the same as the first or second embodiment.
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