Black glass ceramic and preparation method thereof

A black glass and ceramic technology, applied in the field of glass ceramic materials, can solve the problems of poor quality of production process, low yield and high technical requirements, and achieve the effects of cost saving, less pollution and stable color.

Inactive Publication Date: 2015-12-09
GUANGXI NANNING ZHICUI SCI TECH CONSULTATION CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the complex manufacturing process and high technical requirements of glass ceramic panels, the high-quality glass ceramic production process and control technology are basically monopolized by foreign countries, and the domestic glass ceramic production process has problems such as poor quality and low yield.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] A kind of black glass-ceramic, comprises the raw material of following weight parts: 58 parts of mica powders, 18 parts of potassium permanganate, 12 parts of mica powders, 8 parts of copper sulfate pentahydrate, 8 parts of sodium silicate, 22 parts of silicon dioxide, 30 parts of zinc oxide, 6 parts of ammonium polyacrylate.

[0024] Wherein, the particle diameter of silicon dioxide is 250nm, the particle diameter of zinc oxide is 500nm, and the relative molecular mass of ammonium polyacrylate is 1000.

[0025] Prepare the preparation method of above-mentioned black glass-ceramic, comprise the following steps:

[0026] (1) Weigh mica powder, potassium permanganate, mica powder, copper sulfate pentahydrate, sodium silicate, silicon dioxide, zinc oxide and ammonium polyacrylate by weight, mix and add in the pot of oranges;

[0027] (2) Heating the crucible, keeping it at 1500°C for 2 hours, quenching to form a frit, and crushing into glass powder;

[0028] (3) Melt the...

Embodiment 2

[0031] A black glass-ceramic, comprising the following raw materials in parts by weight: 50 parts of mica powder, 12 parts of potassium permanganate, 5 parts of mica powder, 6 parts of copper sulfate pentahydrate, 4 parts of sodium silicate, 16 parts of silicon dioxide, 10 parts of zinc oxide, 3 parts of ammonium polyacrylate.

[0032] Wherein, the particle diameter of silicon dioxide is 350nm, the particle diameter of zinc oxide is 800nm, and the relative molecular mass of ammonium polyacrylate is 5000.

[0033] Prepare the preparation method of above-mentioned black glass-ceramic, comprise the following steps:

[0034] (1) Weigh mica powder, potassium permanganate, mica powder, copper sulfate pentahydrate, sodium silicate, silicon dioxide, zinc oxide and ammonium polyacrylate by weight, mix and add in the pot of oranges;

[0035] (2) Heating the crucible, holding it at 1600°C for 1 hour, quenching to form a frit, and crushing into glass powder;

[0036] (3) Melt the glass ...

Embodiment 3

[0039] A black glass-ceramic, comprising the following raw materials in parts by weight: 70 parts of mica powder, 25 parts of potassium permanganate, 16 parts of mica powder, 12 parts of copper sulfate pentahydrate, 14 parts of sodium silicate, 28 parts of silicon dioxide, 40 parts of zinc oxide, 10 parts of ammonium polyacrylate.

[0040] Among them, the particle size of silicon dioxide is 300nm, the particle size of zinc oxide is 600nm, and the relative molecular mass of ammonium polyacrylate is 3000

[0041] Prepare the preparation method of above-mentioned black glass-ceramic, comprise the following steps:

[0042] (1) Weigh mica powder, potassium permanganate, mica powder, copper sulfate pentahydrate, sodium silicate, silicon dioxide, zinc oxide and ammonium polyacrylate by weight, mix and add in the pot of oranges;

[0043] (2) Heating the crucible, holding it at 1550°C for 1.5h, quenching to form a frit, and crushing into glass powder;

[0044] (3) Melt the glass powd...

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PUM

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Abstract

The invention discloses black glass ceramic and a preparation method thereof. The ceramic is prepared from, by weight, 50-70 parts of mica powder, 12-25 parts of potassium permanganate, 5-16 parts of mica powder, 6-12 parts of blue vitriol, 4-14 parts of sodium silicate, 16-28 parts of silicon dioxide, 10-40 parts of zinc oxide and 3-10 parts of ammonium polyacrylate. The preparation method of the black glass ceramic comprises the steps of weighing raw materials according to the parts by weight, mixing and adding the raw materials into a crucible, heating the crucible, keeping temperature retention for 1-2 hours within the range from 1500 DEG C to 1600 DEG C, conducting shocking chilling, forming frit, smashing the frit into glass powder, placing the glass powder into a crucible at the temperature ranging from 1050 DEG C to 1100 DEG C for fusion, conducting natural cooling, and obtaining the black glass ceramic. According to the formula of the black glass ceramic, the mixing is conducted according to a certain proportion, then the black glass ceramic is obtained and is in black, products obtained after the mixing are stable in color and luster, little pollution is caused in the production process, only traditional ceramic firing equipment is needed for production, no additional dedicated electroplating equipment is needed, and the cost is saved.

Description

technical field [0001] The invention belongs to the field of glass ceramic materials, and in particular relates to a black glass ceramic and a preparation method thereof. Background technique [0002] Glass-ceramics, also known as glass-ceramic, is a kind of composite material combined with crystal phase and glass made through high-temperature melting, molding, and heat treatment. With high mechanical strength, adjustable thermal expansion, thermal shock resistance, chemical corrosion resistance, low dielectric loss and other superior properties, it is widely used in machinery manufacturing, optics, electronics and microelectronics, aerospace, chemistry, industry, biomedicine and construction and other fields. Due to the complex manufacturing process and high technical requirements of glass ceramic panels, the high-quality glass ceramic production process and control technology are basically monopolized by foreign countries, and the domestic glass ceramic production process...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C6/04
Inventor 黄能强
Owner GUANGXI NANNING ZHICUI SCI TECH CONSULTATION CO LTD
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