Preparation method for lithium iron phosphate cathode slurry
A technology of lithium iron phosphate and cathode slurry, which is applied in battery electrodes, electrical components, circuits, etc., can solve the problems of performance impact of pole piece lithium batteries, long-term treatment of conductive agents, equipment requirements and high wear and tear, and achieves short preparation time. , The effect of small equipment wear and low production energy consumption
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Embodiment 1
[0026] Use SP as conductive agent, PVDF as binder, according to LiFePO 4 : SP:PVDF=95.7:2.3:2.0 mass ratio, solvent NMP is 100% of the total amount of each component. The preparation steps are as follows:
[0027] 1. Add the components to the mixing tank and stir and disperse for 40 minutes, and scrape the powder on the mixing paddle and the tank at the time of 20 minutes and 40 minutes;
[0028] 2. Add 55% of the total amount of NMP to the above-mentioned stirred powder, stir and disperse for 70 minutes, and scrape the slurry on the stirring paddle and the barrel at the time of 20 minutes, 40 minutes and 60 minutes. The temperature of the slurry is controlled between 25~35℃;
[0029] 3. Add 35% of the total amount of solvent to the above-mentioned high-viscosity stirred slurry, stir and disperse for 60 minutes, and scrape the slurry on the stirring paddle and the barrel at the time of 23 minutes, 46 minutes and 70 minutes. The temperature of material and slurry is controlled betwe...
Embodiment 2
[0037] Use SP and KS-6 as conductive agent, PVDF as binder, according to LiFePO 4 : SP:KS-6:PVDF=93:2.2:1.3:3.5 mass ratio, solvent NMP is 120% of the total amount of the above components. The preparation steps are as follows:
[0038] 1. Add each component to the mixing tank and stir and disperse for 30 minutes. At the time of 15 minutes and 30 minutes, scrape the powder on the mixing paddle and the barrel;
[0039] 2. Add 60% of the total amount of NMP to the above-mentioned stirred powder, stir and disperse for 60 minutes, and scrape the slurry on the stirring paddle and the barrel at the time of 20 minutes, 40 minutes and 60 minutes. The temperature of the slurry is controlled between 25~35℃;
[0040] 3. Add 30% of the total amount of solvent to the above-mentioned high-viscosity stirred slurry, stir and disperse for 60 minutes, and scrape the slurry on the stirring paddle and the barrel at the time of 20 minutes, 40 minutes and 60 minutes The temperature of material and slurry...
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