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A kind of high elongation silicone sealant and preparation method thereof

A silicone sealant, high elongation technology, used in adhesives, non-polymer adhesive additives, adhesive additives, etc. problems, to achieve the effect of long service life, strong weather resistance and simple process

Active Publication Date: 2018-02-09
RIFENG ENTERPRISE FOSHAN CO LTD +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] 1. α, ω-dihydroxypolydimethylsiloxane (referred to as 107 glue) is generally used as the base glue for ordinary silicone glue on the market, and there is no chain extension reaction. The elasticity and elongation of the prepared silicone glue Low, resulting in poor displacement resistance of the sealant;

Method used

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  • A kind of high elongation silicone sealant and preparation method thereof
  • A kind of high elongation silicone sealant and preparation method thereof
  • A kind of high elongation silicone sealant and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0031] A high-elongation silicone sealant, in parts by mass, comprising the following raw materials: 25 parts of α, ω-dimethoxy polydimethylsiloxane with a viscosity of 0.5 million centipoise, and a viscosity of 60 centipoise 1.8 parts of DL-400, 22 parts of base material, 6.5 parts of fumed silica, 39 parts of quartz powder, 4.2 parts of methyltrimethoxysilane, 0.8 parts of primary titanium, 0.5 parts of secondary titanium, γ-(2,3 - 0.14 parts of glycidyloxy) propyltrimethoxysilane, 0.06 part of dibutyltin dilaurate, the silicone sealant proposed by the present invention can greatly improve the displacement resistance, and can be used for long-term aluminum curtain wall joints, highways, Bridges, airports and other concrete pavement gaps, caulking and sealing of expansion joints and other construction occasions, and the effective use period of the sealant is longer.

[0032] In parts by mass, the base material is composed of 50 parts of methyl silicone oil with a viscosity of...

Embodiment 2

[0043] A high-elongation silicone sealant, in parts by mass, comprising the following raw materials: 65.4 parts of α, ω-dimethoxy polydimethylsiloxane with a viscosity of 250,000 centipoise and a viscosity of 600 centipoise 0.2 parts of DL-30000, 8 parts of base material, 2.5 parts of fumed silica, 18 parts of quartz powder, 2.5 parts of vinyltrimethoxysilane, 1.6 parts of primary titanium, 1.2 parts of secondary titanium, γ-(2,3 -Glycidoxy) propylmethyl dimethoxysilane, γ-aminopropyltriethoxysilane, 0.58 parts of mixed coupling agent of γ-aminopropylmethyldimethoxysilane, dibutyl Tin diacetate 0.02 parts, the silicone sealant proposed by the present invention can greatly improve the displacement resistance, and can be used for long-term use in aluminum curtain wall joints, gaps in concrete roads such as expressways, bridges, airports, caulking and sealing of expansion joints, etc. Construction occasions, and the effective use period of the sealant is longer.

[0044] In part...

Embodiment 3

[0055] A high-elongation silicone sealant, in parts by mass, comprising the following raw materials: 39.2 parts of α, ω-dimethoxy polydimethylsiloxane with a viscosity of 50,000 centipoise and a viscosity of 70 centipoise 0.55 parts of DL-4000, 19.6 parts of base material, 2.9 parts of fumed silica, 32.4 parts of quartz powder, 2.9 parts of vinyl triethoxysilane and methyl triethoxysilane mixed crosslinking agent, 1.2 parts of primary titanium , 0.9 parts of secondary titanium, 0.3 parts of γ-mercaptopropyl trimethoxysilane, 0.3 parts of mixed coupling agent of γ-mercaptopropyl triethoxysilane, 0.05 parts of stannous octoate, the silicone sealant proposed by the present invention, greatly It can improve the anti-displacement ability, and can be used for long-term construction occasions such as joints of aluminum curtain walls, joints of concrete roads such as highways, bridges, and airports, and caulking of expansion joints, and the effective use period of the sealant is longer...

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Abstract

The invention relates to a high-elongation silicone sealant, which comprises the following raw materials in parts by mass: α,ω-dimethoxy polydimethylsiloxane with a viscosity of 0.5-250,000 centipoise 25 to 65.4 parts, 0.2 to 1.8 parts of polyether polyol chain extender with a viscosity of 60 to 600 centipoise, 8 to 22 parts of base material, 20.5 to 45.5 parts of filler, 2.5 to 4.2 parts of crosslinking agent, 0.8 to 0.8 parts of primary titanium 1.6 parts, 0.5-1.2 parts of secondary titanium, 0.14-0.58 parts of coupling agent, 0.02-0.06 parts of catalyst, the base material is composed of methyl silicone oil with a viscosity of 50-1500 centistokes, active calcium carbonate with a particle size of 20-100nm and hydroxyl scavenger composition. The silicon-copper sealant provided by the invention can improve the anti-displacement ability, and is used in construction occasions such as aluminum plate curtain wall joints, bridges, airport concrete pavement gaps, caulking and sealing of expansion joints, etc., and the effective service life of the sealant is longer.

Description

technical field [0001] The invention belongs to the technical field of silicone sealants, and in particular relates to a high-elongation silicone sealant and a preparation method thereof. Background technique [0002] Organic silicone sealant is a polymer compound with Si-O bond three-dimensional network structure, its Si-O bond energy is as high as 425KJ / mol, good stability, strong weather resistance, excellent stain resistance, high Low temperature, good hydrophobicity and air permeability, etc., can be used for a long time in the range of -60 ~ 200 ℃, so its application field is also expanding, and has gradually expanded from the field of construction to the fields of automobiles, aviation, aerospace and marine engineering. middle. [0003] Since the 1980s, with the prefabrication and high-rise construction of domestic buildings and the extensive use of flexible structures of glass and metal curtain walls and large-scale frame-type hanging panel structures, a large numbe...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09J183/14C09J183/04C09J11/04C09J11/06
Inventor 邓叔元张升袁昆鹏
Owner RIFENG ENTERPRISE FOSHAN CO LTD
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