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Hot melt adhesive for acrylic hot-fix rhinestone and preparation method thereof

An acrylic hot-drilling and hot-melt adhesive technology, which is applied in the direction of adhesives, adhesive types, mineral oil-hydrocarbon copolymer adhesives, etc. Acrylic hot drilling and other problems, to achieve the effect of good optical performance, wide range of hardness, resistance to environmental stress cracking

Active Publication Date: 2016-01-27
HUANGSHAN XINDECHENG GLUE IND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, when the above-mentioned hot melt adhesive is used for hot-drilling products, its shear peel strength is low, the tensile strength is not enough, and it is easy to peel off, which cannot meet the requirements of hot-drilling products.
[0004] At present, the hot-melt adhesives used for ironing drills are mainly polyamide hot-melt adhesives and EVA resin hot-melt adhesives. Polyamide hot-melt adhesives have a high pressing temperature and are easy to burn acrylic hot-melt drills. The operation is difficult and the bonding strength is difficult. Meet the requirements

Method used

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  • Hot melt adhesive for acrylic hot-fix rhinestone and preparation method thereof
  • Hot melt adhesive for acrylic hot-fix rhinestone and preparation method thereof
  • Hot melt adhesive for acrylic hot-fix rhinestone and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Embodiment 1: The present invention provides the composition and preparation method thereof of hot-melt adhesive

[0027] Add 14 parts by weight of polyethylene wax to the ribbon-stirred hot-melt adhesive reaction kettle, heat it to 160°C, and after it is completely melted, add 11 parts by weight of EVA resin (VA content is 28%, MI: 150g / 10min) , the EVA resin of 22 parts by weight (VA content is 28%, MI:6g / 10min), the antioxidant 1010 of 1 part by weight, the thermoplastic polyurethane of 8 parts by weight, the ethylene-butyl acrylate copolymer EBA3427AC of 4 parts by weight, Under the protection of nitrogen, control the temperature at 180°C, stir for 2 hours, add 40 parts by weight of styrene-modified C5 petroleum resin, control the temperature at 160°C, stir for 1 hour, vacuumize, enter the strip, cooling, Pelletizing process, hot-melt hot melt adhesive S1 can be obtained.

Embodiment 2

[0028] Embodiment 2: The present invention provides the composition and preparation method thereof of hot-melt adhesive

[0029] Add 20 parts by weight of polyethylene wax to the ribbon-stirred hot-melt adhesive reaction kettle, heat it to 160°C, and add 15 parts by weight of EVA resin (VA content: 28%, MI: 150g / 10min) after melting is complete , the EVA resin of 30 parts by weight (VA content is 28%, MI:6g / 10min), the antioxidant 1010 of 1 part by weight, the thermoplastic polyurethane of 8 parts by weight, the ethylene-butyl acrylate copolymer EBA3427AC of 2 parts by weight, Under the protection of nitrogen, control the temperature at 180°C, stir for 2 hours, add 40 parts by weight of styrene-modified C5 petroleum resin, control the temperature at 160°C, stir for 1 hour, vacuumize, enter the strip, cooling, Pelletizing process, that is hot-melt hot melt adhesive S2.

Embodiment 3

[0030] Embodiment 3: The present invention provides the composition and preparation method thereof of hot-melt adhesive for ironing diamonds

[0031] Add 10 parts by weight of polyethylene wax to the ribbon-stirred hot-melt adhesive reaction kettle, heat it to 160°C, and after it is completely melted, add 11 parts by weight of EVA resin (VA content is 28%, MI: 150g / 10min) , the EVA resin of 26 parts by weight (VA content is 28%, MI:6g / 10min), the antioxidant 1010 of 1 part by weight, the thermoplastic polyurethane of 4 parts by weight, the ethylene-butyl acrylate copolymer EBA3427AC of 4 parts by weight, Under the protection of nitrogen, control the temperature at 180°C, stir for 2 hours, add 40 parts by weight of styrene-modified C5 petroleum resin, control the temperature at 160°C, stir for 1 hour, vacuumize, enter the strip, cooling, The pelletizing process yields hot-melt hot melt adhesive S3.

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Abstract

The invention provides a hot melt adhesive for an acrylic hot-fix rhinestone. The hot melt adhesive comprises the following components by weight: 10 to 15 parts of EVA resin with the VA content of 28% and the MI of 150 g / 10min, 0 to 35 parts of EVA resin with the VA content of 28% and the MI of 6 g / 10min, 4 to 12 parts of thermoplastic polyurethane with Shore D hardness of 70, 30 to 40 parts of styrene modified C5 petroleum resin, 10 to 20 parts of polyethylene wax, 2 to 6 parts of EBA3427AC and 1 to 2 parts of an antioxidant 1010. The hot melt adhesive for the acrylic hot-fix rhinestone provided by the invention has a hot-press temperature of 115 to 120 DEG C, is not prone to scalding the acrylic hot-fix rhinestone and fabrics, and has peeling strength of no less than 4.0kN / m , thereby having high bonding strength at the same time; meanwhile, the hot melt adhesive has the advantage of good adhesive force with a variety of fabrics and acrylic hot-fix rhinestones, and is an ideal hot melt adhesive for the acrylic hot-fix rhinestone.

Description

technical field [0001] The invention belongs to hot-melt adhesives and a preparation method thereof, in particular to acrylic hot-melt hot-melt adhesives and a preparation method thereof. Background technique [0002] Acrylic hot-melt adhesive is a kind of hot-melt adhesive coated on the back of acrylic hot-melt after heating and melting. Melt glue plays the role of bonding ironing diamonds and clothing fabrics, and is also suitable for various materials of luggage and footwear. The hot melt adhesive is required to have a softening point suitable for hot drilling, high peel strength, and water washing resistance. [0003] For example, CN102703006A discloses a hot-melt adhesive, which specifically relates to a kind of strong adhesive force, fast drying speed, small consumption, good thermal stability, anti-aging, anti-acid and alkali, pollution-free and adaptable to high-speed automatic assembly line production packaging The required hot melt adhesive and its preparation me...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09J157/02C09J123/08C09J175/04C09J123/06
Inventor 王峰汪十荣汪岩
Owner HUANGSHAN XINDECHENG GLUE IND CO LTD
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