Metal-surface composite protective layer and preparing method thereof
A metal protection and metal surface technology, applied in metal material coating technology, coating, gaseous chemical plating, etc., can solve the problems of easy-to-corrosion metal and RTV coating adhesion, etc., to achieve good insulation and corrosion resistance, high thermal conductivity performance, excellent insulation, anti-corrosion and surface self-cleaning properties
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[0011] A method for preparing a metal protective layer, comprising the following steps: a. Substrate preparation: polishing the copper substrate, polishing the copper substrate sequentially with different types of sandpaper, and then polishing the surface with diamond abrasive paste; then using acetone, anhydrous Ultrasonic cleaning was performed with ethanol and deionized water for 10 minutes each to remove residual particles and impurities on the surface until the surface of the copper substrate was clean, and then dried with nitrogen.
[0012] b. Film deposition: Spray silicon oxide film on the prepared substrate by using atmospheric pressure plasma jet.
[0013] c. Coating RTV paint: the copper substrate treated in step 2 is coated with a layer of RTV paint by brushing, and after drying for 48 hours, a flat and smooth paint film is obtained, and silicon oxides of different thicknesses are obtained. RTV coating composite protective layer.
example 1
[0015] Example 1 uses metal copper as the substrate, attaches a silicon oxide film with a thickness of 0.5mm, and coats RTV paint with a thickness of 0.3mm
[0016] Determination of contact resistance - contact resistance per unit area 0.146Ω / ㎝ 2
[0017] Volume resistivity ≥ 2.0×1014Ω·㎝
[0018] Impulse current withstand test - diffuse current is 23.8KA
[0019] Breakdown voltage 18~25kv / mm
[0020] Dielectric constant 3.0 / 60HZ
[0021] Adhesion Test - Level 1
[0022] Heat resistance No cracking for 1000 hours at 85°C in a thermostat
[0023] Corrosion resistance (5% salt spray test for 120 hours) no rust
example 2
[0024] Example 2 uses metal copper as the base, attaches a silicon oxide film with a thickness of 0.5mm, and coats RTV paint with a thickness of 0.5mm
[0025] Contact resistance - contact resistance per unit area 2.72Ω / ㎝ 2
[0026] Volume resistivity ≥ 2.0×1014Ω·㎝
[0027] Impulse current withstand test - diffuse current is 23.8KA
[0028] Breakdown voltage 18~25kv / mm
[0029] Dielectric constant 3.0 / 60HZ
[0030] Adhesion Test - Level 1
[0031] Heat resistance No cracking for 1000 hours at 85°C in a thermostat
[0032] Corrosion resistance (5% salt spray test for 120 hours) no rust
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