A preparation method of cotton fabric with conductive, electromagnetic shielding and flame retardant functions
An electromagnetic shielding and cotton fabric technology, which is applied in the field of functional cotton fabric preparation, can solve the problems of loss of electrical conductivity, easy de-doping of doping acid, etc., and achieves the effects of improving stability, not easy to de-doping, and high affinity
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Embodiment 1
[0011] (1) Dissolve 3mL tetraethyl orthosilicate in 50mL absolute ethanol, add 3mL ammonia water, stir at 60ºC for 30min to obtain a milky white solution;
[0012] (2) Cool the above solution to room temperature, and add 1 mL of pyrrole;
[0013] (3) Soak the cotton fabric in the mixed solution of step 2 for 20 minutes, two dipping and two rolling, and the rolling rate is 90%;
[0014] (4) Soak the padded cotton fabric in an aqueous solution containing 2g ammonium persulfate, 5g phytic acid and 0.1mL silane coupling agent KH560 for 1 hour, and roll off the excess aqueous solution on a paddle;
[0015] (5) Dry the above cotton fabric at 60ºC, then bake at 120ºC for 3 minutes, and finally wash and dry.
Embodiment 2
[0017] (1) Dissolve 4mL tetraethyl orthosilicate in 50mL absolute ethanol, add 4mL ammonia water, and stir at 60ºC for 30min to obtain a milky white solution;
[0018] (2) Cool the above solution to room temperature, and add 3 mL of pyrrole;
[0019] (3) Immerse the cotton fabric in the mixed solution of step 2 for 15 minutes, two dipping and two rolling, and the rolling rate is 100%;
[0020] (4) Soak the padded cotton fabric in 100mL aqueous solution containing 6g ammonium persulfate, 7g phytic acid and 0.2mL silane coupling agent KH560 for 1 hour, and roll off the excess aqueous solution on a paddle car;
[0021] (5) Dry the above cotton fabric at 60ºC, then bake at 120ºC for 4 minutes, and finally wash and dry.
Embodiment 3
[0023] (1) Dissolve 5mL tetraethyl orthosilicate in 50mL absolute ethanol, add 5mL ammonia water, stir at 60ºC for 30min to obtain a milky white solution;
[0024] (2) Cool the above solution to room temperature, and add 5 mL of pyrrole;
[0025] (3) Soak the cotton fabric in the mixed solution of step 2 for 20 minutes, two dipping and two rolling, and the rolling rate is 90%;
[0026] (4) Soak the padded cotton fabric in 100mL aqueous solution containing 7g ammonium persulfate, 10g phytic acid and 0.3mL silane coupling agent KH560 for 1 hour, and roll off the excess aqueous solution on a paddle car;
[0027] (5) Dry the above cotton fabric at 60ºC, then bake at 120ºC for 5 minutes, and finally wash and dry.
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