Composite toughened grouting cement mortar and preparation method thereof
A cement mortar and toughening technology, applied in the field of building materials, can solve the problems of application limitation, easy cracking, large internal stress, etc., and achieve the effects of easily satisfying preparation conditions, reducing maintenance costs, and improving crack resistance.
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Embodiment 1
[0044] 1. Preparation of modified composite carbon nanomaterials:
[0045] 1) Put 62 stainless steel balls with a diameter of 5mm and 46 stainless steel balls with a diameter of 10mm in two identical 6L nylon ball mill tanks, and then add 1.4kg of natural single crystal graphite powder and multi-walled carbon nanotubes respectively According to the composite carbon material with a mass ratio of 1.5:1, 120mL of absolute ethanol was added dropwise, sealed with a nylon cover, and two ball mill jars were symmetrically placed in the ball mill. Under the condition of ball milling for 60h;
[0046] 2) Add the composite carbon material treated in step 1) into Tween40 aqueous solution with a pH value of 8 and a mass concentration of 16%, ultrasonication for 15 hours, and filtration. The resulting filter residue was washed with water and then vacuum-dried at 62°C for 20 hours;
[0047] 3) Add the composite carbon material treated in step 2) into the HCl solution with a concentration of...
Embodiment 2
[0060] 1. Preparation of modified composite carbon nanomaterials:
[0061] 1) Put 62 stainless steel balls with a diameter of 5mm and 46 stainless steel balls with a diameter of 10mm into two identical 6L nylon ball mill tanks, and then add 1.4kg of high-purity ultrafine graphite powder and multi-walled carbon nanotubes. Composite carbon material with a mass ratio of 1.5:1, then add 120mL of absolute ethanol dropwise, seal it with a nylon cover, put two ball mill jars into the ball mill symmetrically, at a speed of 500rpm, and automatically change the direction of rotation every 30min Lower ball milling treatment for 60h;
[0062] 2) Add the composite carbon material treated in step 1) into Tween40 aqueous solution with a pH value of 8 and a mass concentration of 16%, ultrasonication for 15 hours, and filtration. The resulting filter residue was washed with water and then vacuum-dried at 62°C for 20 hours;
[0063] 3) Add the composite carbon material treated in step 2) into ...
Embodiment 3
[0076] 1. Preparation of modified composite carbon nanomaterials:
[0077] 1) Put 62 stainless steel balls with a diameter of 5mm and 46 stainless steel balls with a diameter of 10mm into two identical 6L nylon ball mill tanks, and then add 1.4kg of high-purity ultrafine graphite powder and multi-walled carbon nanotubes. Composite carbon material with a mass ratio of 1.5:1, then add 120mL of absolute ethanol dropwise, seal it with a nylon cover, put two ball mill jars into the ball mill symmetrically, at a speed of 500rpm, and automatically change the direction of rotation every 30min Lower ball milling treatment for 60h;
[0078] 2) Add the composite carbon material treated in step 1) into Tween40 aqueous solution with a pH value of 8 and a mass concentration of 16%, ultrasonication for 15 hours, and filtration. The obtained filter residue was washed with water and then vacuum-dried at 60°C for 20 hours;
[0079] 3) Add the composite carbon material treated in step 2) into t...
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