Field emission cathode and its preparation method and application
A field emission cathode and conductive substrate technology, which is applied in the field emission field, can solve problems such as application limitations, poor emission stability, and small emission current, and achieve the effects of reducing production costs, stable performance, and reducing contact resistance
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[0032] On the other hand, on the basis of the field emission cathode of the embodiment of the present invention described above, the embodiment of the present invention also provides a preparation method of the field emission cathode of the embodiment of the present invention. The preparation method of the field emission cathode of the embodiment of the present invention is as follows figure 2 Therefore, see also figure 1 , its preparation method comprises the following steps:
[0033] S01. Forming a graphene layer 2 on the surface of the conductive substrate 1;
[0034] S02. Electrophoretic deposition of molybdenum disulfide and / or tungsten disulfide nanosheet layer 3 on the surface of graphene layer 2:
[0035] Molybdenum disulfide and / or tungsten disulfide nanosheets and charge additives are dispersed in an organic solvent to form an electrophoretic solution, the conductive substrate is used as a negative electrode, and under the action of an external electric field, the m...
Embodiment 1
[0059] The embodiment of the present invention provides a field emission cathode and a preparation method thereof. Among them, the field emission cathode structure such as figure 1 As shown, it includes a conductive substrate 1 / graphene layer 2 / molybdenum disulfide nanosheet layer 3 sequentially stacked and combined. Wherein, the conductive substrate 1 material is a copper sheet; the thickness of the graphene layer 2 is 5nm; The thickness is 3-5 μm.
[0060] Its preparation method is as follows:
[0061] S11. Provide conductive substrate: copper sheet
[0062] S12. chemical vapor deposition (CVD) method growth graphene layer:
[0063] Put the conductive substrate coated with the catalyst metal layer into the reaction furnace, pass in argon (Ar), heat the substrate to the reaction temperature of 900 ° C, keep it warm for a period of time, and then pass in methane and hydrogen (H 2 ) mixed gas to grow graphene nanosheets for 5min. After the reaction was over, it was cooled ...
Embodiment 2
[0068] The embodiment of the present invention provides a field emission cathode and a preparation method thereof. Among them, the field emission cathode structure such as figure 1 As shown, it includes a conductive substrate 1 / graphene layer 2 / molybdenum disulfide nanosheet layer 3 sequentially stacked and combined. Among them, the material of conductive substrate 1 is n-type doped silicon sheet; the thickness of graphene layer 2 is 10nm; The thickness of the molybdenum nanosheet layer 3 is 8-10 μm.
[0069] Its preparation method is as follows:
[0070] S21. Provide conductive substrate: n-type doped silicon wafer
[0071] S22. chemical vapor deposition (CVD) method growth graphene layer:
[0072] Put the conductive substrate coated with the catalyst metal layer into the reaction furnace, pass in argon (Ar), heat the substrate to the reaction temperature of 900 ° C, keep it warm for a period of time, and then pass in methane and hydrogen (H 2 ) mixed gas to grow graphen...
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