Textile printing thickening agent and production process thereof

A production process and technology for textiles, applied in the field of textile printing thickeners, can solve problems such as adverse environmental effects, intolerant electrolytes, and large energy consumption, achieve good dispersibility and surface activity, strong electrolyte resistance, and optimize production processes. Effect

Inactive Publication Date: 2016-07-06
HEFEI JUHE RADIAL CHEM TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Traditional thickeners consume a lot of energy in the production process, and produce APEO at the same time, which has a negative impact on the environment. Moreover, the products are not resistant to electrolytes, use a large amount, and the cost of use is high. The printed textiles are dark in color and feel poor.
However, natural polymer pastes such as sodium alginate have the disadvantages of long pulping cycle and easy mildew of the prepared pulp.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0059] The textile printing thickener is prepared by processing the following raw materials in parts by weight:

[0060] 150 parts of acrylic

[0061] 20 parts of methacrylic acid

[0062] 50 parts of acrylamide

[0063] 1 part of octadecyl acrylate

[0064] 0.01 part of N-N’ methylene bisacrylamide

[0065] 120 copies of white oil or jet fuel

[0066] 15 parts of sorbitan monooleate

[0067] 0.2 parts of initiator

[0068] 0.01 part of sodium bisulfite

[0069] Fatty alcohol polyoxyethylene ether 10 parts

[0070] 5 parts of hydrophilic silicone oil

[0071] 200 parts of sodium hydroxide solution.

[0072] The ratio of the mass of sodium hydroxide in the sodium hydroxide solution to the total mass of the solution is 28%. The initiator is potassium persulfate.

[0073] The production process of textile printing thickener includes the following steps:

[0074] 1) Neutralize the above-mentioned acrylic acid and methacrylic acid in parts by weight with sodium hydroxide solution to pH 5.2;

[0075] 2...

Embodiment 2

[0080] The textile printing thickener is prepared by processing the following raw materials in parts by weight:

[0081] 220 parts of acrylic

[0082] 60 parts of methacrylic acid

[0083] 80 parts of acrylamide

[0084] 10 parts of octadecyl acrylate

[0085] 0.5 part of N-N’ methylene bisacrylamide

[0086] 250 copies of white oil or jet fuel

[0087] 50 parts of sorbitan monooleate

[0088] 2 parts of initiator

[0089] 1 part of sodium bisulfite

[0090] Fatty alcohol polyoxyethylene ether 50 parts

[0091] 50 parts of hydrophilic silicone oil

[0092] 500 parts of sodium hydroxide solution.

[0093] The ratio of the mass of sodium hydroxide in the sodium hydroxide solution to the total mass of the solution is 35%. The initiator is sodium persulfate.

[0094] The production process of textile printing thickener includes the following steps:

[0095] 1) Neutralize the above-mentioned acrylic acid and methacrylic acid in parts by weight with sodium hydroxide solution to pH 6.5;

[0096] 2) Add ...

Embodiment 3

[0101] The textile printing thickener is prepared by processing the following raw materials in parts by weight:

[0102] 180 parts of acrylic

[0103] 40 parts of methacrylic acid

[0104] 60 parts of acrylamide

[0105] 5 parts of octadecyl acrylate

[0106] 0.2 part of N-N’ methylene bisacrylamide

[0107] 150 copies of white oil or jet fuel

[0108] 30 parts of sorbitan monooleate

[0109] 1 part of initiator

[0110] 0.5 part of sodium bisulfite

[0111] 30 parts of fatty alcohol polyoxyethylene ether

[0112] 30 parts of hydrophilic silicone oil

[0113] 300 parts of sodium hydroxide solution.

[0114] The ratio of the mass of sodium hydroxide in the sodium hydroxide solution to the total mass of the solution is 30%. The initiator is a mixture selected from potassium persulfate and sodium persulfate.

[0115] The production process of textile printing thickener includes the following steps:

[0116] 1) Neutralize the above-mentioned acrylic acid and methacrylic acid in parts by weight with ...

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PUM

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Abstract

The invention discloses a textile printing thickening agent. The textile printing thickening agent is prepared by processing the following raw materials in parts by weight: 150-220 parts of acrylic acid, 20-60 parts of methacrylic acid, 50-80 parts of acrylamide, 1-10 parts of octadecyl acrylate, 0.01-0.5 part of N,N'-methylene-bisacrylamide, 120-250 parts of white oil or aviation kerosene, 15-50 parts of sorbitan monooleate, 0.2-2 parts of an initiator, 0.01-1 part of sodium hydrogensulfite, 10-50 parts of fatty alcohol polyoxyethylene ether, 5-50 parts of hydrophilic silicon oil and 200-500 parts of a sodium hydroxide solution. The thickening agent has good water holding performance, strong electrolyte resistance capability and high color yield. A production process comprises the following steps of: (1) neutralizing the acrylic acid and the methacrylic acid until the pH value is 5.2-6.5; (2) adding the acrylamide, the N,N'-methylene-bisacrylamide and the initiator to prepare a water phase; (3) mixing the white oil or the aviation kerosene, the sorbitan monooleate and the octadecyl acrylate to form an oil phase; and (4) adding the water phase into the oil phase and emulsifying, and adding sodium hydrogensulfite to carry out a polymerization reaction; and (5) adding the fatty alcohol polyoxyethylene ether and the hydrophilic silicon oil and mixing.

Description

Technical field [0001] The invention relates to a textile printing thickener and its production process. Background technique [0002] Traditional thickeners consume a lot of energy during the production process, and at the same time produce APEO, which has a negative impact on the environment, and the product is not resistant to electrolytes, the usage is large, the use cost is high, the printed textiles are dark in color and have poor hand feeling . However, natural polymer pastes such as sodium alginate have disadvantages such as long pulping cycle and easy mildew of the prepared pulp. Summary of the invention [0003] The technical problem to be solved by the present invention is to provide a textile printing thickener with good water holding capacity, strong electrolyte resistance and high color yield. [0004] The textile printing thickener provided by the present invention is prepared by processing the following raw materials in parts by weight: [0005] Acrylic 150-220 pa...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/52D06P1/613C08F220/06C08F220/56C08F220/18C08F222/38
CPCC08F220/06D06P1/5257D06P1/5292D06P1/613C08F220/56C08F220/1818C08F222/385
Inventor 王雪原王冬谢伟杨明虎
Owner HEFEI JUHE RADIAL CHEM TECH
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