Preparation method of rare earth transition alloy rotary target for film coating of magneto-optical recording medium and prepared target of rare earth transition alloy rotary target
A magneto-optical recording and rotating target technology, applied in metal material coating process, sputtering coating, ion implantation coating and other directions, can solve the problems of uneven alloy composition, composition segregation, high oxygen content, and reduce the subsequent process. , reduce production costs, overcome the effect of component segregation
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Embodiment 1
[0022] This embodiment is a method for preparing a (NdDy)(FeCo) rotating target, comprising the following steps:
[0023] (1) Nd23Dy77 (indicating that the atomic ratio of Nd and Dy is 23:77; hereinafter all expressed as such) the rare earth metal alloy block is broken into a particle size of 400 microns, and the Fe80.5Co19.5 transition metal alloy block is broken into a particle size of 200 microns ;Put Nd10, Dy35, Fe44, Co11 (Nd, Dy, Fe, Co atomic ratio is 10:35:44:11) powder into the crucible and heat to 1540°C, keep it warm for 2 hours, then cool down to 1260°C, put Nd23Dy77 and Put the Fe80.5Co19.5 powder into the molten Nd10Dy35Fe44Co11 alloy in the crucible. Since the melting point of the Nd23Dy77 alloy is 1400°C and that of the Fe80.5Co19.5 alloy is 1530°C, they will not melt in the crucible at 1260°C. The original alloying method exists to produce rare earth transition metal alloys.
[0024] (2) Under vacuum, pour the molten rare earth transition metal alloy into a m...
Embodiment 2
[0031] This embodiment is a method for preparing a (PrTb)(FeCo) rotating target, comprising the following steps:
[0032] (1) The Pr30Tb70 rare earth metal alloy block is broken into a particle size of 500 microns, and the Fe65.5Co34.5 transition metal alloy block is broken into a particle size of 250 microns; Pr15, Tb40, Fe25, Co20 powder is put into a crucible and heated to 1570 ° C, Keep warm for 2 hours, then cool down to 1240°C, put Pr23Tb77 and Fe66.5Co34.5 powder into the molten Pr15Tb40Fe25Co20 alloy in the crucible, since the melting point of Pr30Tb70 alloy is 1370°C, and Fe65.5Co34.5 alloy is 1530°C. They will not melt into the crucible at 1240°C, and they still exist in the original alloy form, making rare earth transition metal alloys.
[0033] (2) Under vacuum, pour the molten rare earth transition metal alloy into a mold for molding, and demould after cooling.
[0034] (3) Put the poured target tube into the hot isostatic pressing with argon as the medium, the p...
Embodiment 3
[0040] This embodiment is a method for preparing a (SmGd)(FeCo) rotating target, comprising the following steps:
[0041] (1) The Sm35Gd65 rare earth metal alloy block is broken into a particle size of 550 microns, and the Fe70.5Co29.5 transition metal alloy block is broken into a particle size of 200 microns; Sm12, Gd39, Fe32, Co17 powders are put into a crucible and heated to 1580 ° C, Keep warm for 1.5 hours, then cool down to 1220°C, put Sm35Gd65 and Fe70.5Co29.5 powder into the molten Sm12Gd39Fe32Co17 alloy in the crucible, since the melting point of Sm35Gd65 alloy is 1270°C, and Fe70.5Co29.5 alloy is 1530°C, in They will not melt into the crucible at 1220°C, and still exist in the original alloy form, making rare earth transition metal alloys.
[0042] (2) Under vacuum, pour the molten rare earth transition metal alloy into a mold for molding, and demould after cooling.
[0043] (3) Put the poured target tube into the hot isostatic pressing with argon as the medium, the...
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