Carbon fiber reinforced ethylene-propylene-diene monomer rubber anti-ablation material and preparation method

A technology of EPDM rubber and carbon fiber, which is applied in the field of thermal insulation materials for solid rocket motors, can solve problems such as incompatible chemical interfaces, easy migration of free substances, and interface damage, so as to improve quality, service life, and process matching , the effect of excellent ablation resistance

Active Publication Date: 2016-08-10
HUBEI SANJIANG AEROSPACE JIANGHE CHEM TECH
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  • Application Information

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Problems solved by technology

[0002] Solid rocket motors usually use traditional rubber-based insulation materials. In order to solve the problem that the material decomposes while peeling off and cannot form a carbonized layer of the material, a fixed-length carbon fiber (tile) reinforced phenolic modified nitrile rubber insulation material and braided carbon fiber have been developed. Reinforced phenolic modified nitrile rubber insulation material
This type of material has superior performance, but its matrix material is a polar system. Although transitional resins can be used to achieve bonding with carbon fibers, there is always an incompatible chemical interface, and the internal free substances are easy to migrate to the interface. , forming a phenomenon of enrichment and causing damage to the interface
Thus affecting the quality and service life of the product

Method used

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  • Carbon fiber reinforced ethylene-propylene-diene monomer rubber anti-ablation material and preparation method
  • Carbon fiber reinforced ethylene-propylene-diene monomer rubber anti-ablation material and preparation method
  • Carbon fiber reinforced ethylene-propylene-diene monomer rubber anti-ablation material and preparation method

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Embodiment Construction

[0026] The present invention will be further described below in conjunction with the examples, but the protection scope of the present invention is not limited to the scope expressed in the examples.

[0027] A carbon fiber-reinforced EPDM anti-ablation material, the formulation and component specifications of which are shown in Table 2, and the unit is parts by weight.

[0028]

[0029] Table 2

[0030] The EPDM base material described in the present invention is made of EPDM rubber, white carbon black, stearic acid, triethanolamine, accelerator M, accelerator TMTD, thermoplastic phenolic resin, settled sulfur or DCP, The conventional performance indicators of the prepared EPDM base material after vulcanization must meet the relevant requirements. The vulcanization temperature is 150°C, the time is 1h, and the pressure is 1MPa.

[0031] A method for preparing a carbon fiber reinforced EPDM anti-ablation material, the specific steps are:

[0032] 1) Base material prepara...

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Abstract

The invention discloses a carbon fiber reinforced ethylene-propylene-diene monomer rubber anti-ablation material and a preparation method. The anti-ablation material is prepared from: by weight, 15-30 parts of ethylene-propylene-diene monomer rubber matrix material, 45-50 parts of carbon fiber, and 20-32 parts of phenolic resin. The preparation method includes crushing the matrix material into small pieces, dissolving the material with a solvent to prepare a glue solution, adding the phenolic resin into the glue solution according to the ratio, stirring the mixture fully, distributing the obtained glue solution on the each part of the carbon fiber material uniformly, and air-drying the material. The carbon fiber reinforced ethylene-propylene-diene monomer rubber anti-ablation material can overcome the problems of compatibility and migration, can improve the quality, and can prolong the service life.

Description

technical field [0001] The invention belongs to the technical field of thermal insulation materials for solid rocket motors, and in particular relates to a carbon fiber reinforced EPDM rubber anti-ablation material. Background technique [0002] Solid rocket motors usually use traditional rubber-based insulation materials. In order to solve the problem that the material decomposes while peeling off and cannot form a carbonized layer of the material, fixed-length carbon fiber (tile) reinforced phenolic modified nitrile rubber insulation material and braided carbon fiber have been developed. Reinforced phenolic modified nitrile rubber insulation. This type of material has superior performance, but its matrix material is a polar system. Although transitional resins can be used to achieve bonding with carbon fibers, there is always an incompatible chemical interface, and the internal free substances are easy to migrate to the interface. , forming a phenomenon of enrichment and ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L23/16C08L61/06C08L61/14C08K7/06C08J5/04
CPCC08J5/042C08J2323/16C08J2361/14C08J2423/16C08J2461/14C08L23/16C08L61/14C08L2201/02C08L2205/02C08L2205/03C08K7/06C08L61/06
Inventor 朱稼麟刘美珍李方朔陈永钊曾庆江贾冬梅
Owner HUBEI SANJIANG AEROSPACE JIANGHE CHEM TECH
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