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Tooth filling material and preparation method thereof

A technology for filling materials and teeth, applied in dental preparations, dentistry, dental prosthesis, etc., can solve the problems of poor polishing performance, color and luster, prevent thermal conductivity, etc., achieve excellent polishing performance, prevent edge micro-leakage, and long service life.

Inactive Publication Date: 2016-08-31
SUZHOU COSMETIC MATERIALS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Technical problem to be solved: Aiming at the disadvantages of existing composite resin dental filling materials, such as poor polishing performance, color, and poor heat conduction prevention performance, the present invention provides a dental Filling material and preparation method thereof

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] A tooth filling material, which contains the following components in parts by mass: 15 parts of glycidyl methacrylate, 10 parts of gum arabic, 5 parts of glass powder, 5 parts of silicon dioxide, 3 parts of nano-montmorillonite, and 1 part of calcium carbonate , 0.5 parts of 1,6-hexanediol diacrylate, 0.8 parts of dicumyl peroxide, 0.3 parts of triethylenediamine, 0.2 parts of ethylenediaminetetraacetic acid, 0.2 parts of organotin stabilizer, 3 parts of zinc phosphate cement , 0.1 part of resorcinol monobenzoate.

[0018] A preparation method of tooth filling material, the steps of the preparation method are as follows:

[0019] Step 1: Mix glass powder, silicon dioxide, nano-montmorillonite and calcium carbonate evenly to obtain a mixed powder;

[0020] The second step: 1,6-hexanediol diacrylate, dicumyl peroxide, triethylenediamine, ethylenediaminetetraacetic acid, organotin stabilizer, zinc phosphate cement, resorcinol monobenzoate Mix the esters evenly to obtain ...

Embodiment 2

[0023] A tooth filling material, which contains the following components in parts by mass: 35 parts of glycidyl methacrylate, 25 parts of gum arabic, 20 parts of glass powder, 15 parts of silicon dioxide, 12 parts of nano-montmorillonite, and 6 parts of calcium carbonate , 3 parts of 1,6-hexanediol diacrylate, 3.5 parts of dicumyl peroxide, 1.5 parts of triethylenediamine, 1 part of ethylenediaminetetraacetic acid, 1.2 parts of organotin stabilizer, 10 parts of zinc phosphate cement , 0.5 parts of resorcinol monobenzoate.

[0024] A preparation method of tooth filling material, the steps of the preparation method are as follows:

[0025] Step 1: Mix glass powder, silicon dioxide, nano-montmorillonite and calcium carbonate evenly to obtain a mixed powder;

[0026] The second step: 1,6-hexanediol diacrylate, dicumyl peroxide, triethylenediamine, ethylenediaminetetraacetic acid, organotin stabilizer, zinc phosphate cement, resorcinol monobenzoate Mix the esters evenly to obtain...

Embodiment 3

[0029] A tooth filling material, which contains the following components in parts by mass: 30 parts of glycidyl methacrylate, 22 parts of gum arabic, 16 parts of glass powder, 12 parts of silicon dioxide, 11 parts of nano-montmorillonite, and 5 parts of calcium carbonate , 2.2 parts of 1,6-hexanediol diacrylate, 3 parts of dicumyl peroxide, 1.3 parts of triethylenediamine, 0.8 parts of ethylenediaminetetraacetic acid, 1 part of organotin stabilizer, 9 parts of zinc phosphate cement , 0.4 parts of resorcinol monobenzoate.

[0030] A preparation method of tooth filling material, the steps of the preparation method are as follows:

[0031] Step 1: Mix glass powder, silicon dioxide, nano-montmorillonite and calcium carbonate evenly to obtain a mixed powder;

[0032] The second step: 1,6-hexanediol diacrylate, dicumyl peroxide, triethylenediamine, ethylenediaminetetraacetic acid, organotin stabilizer, zinc phosphate cement, resorcinol monobenzoate Mix the esters evenly to obtain ...

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PUM

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Abstract

The invention relates to a tooth filling material and a preparation method thereof. The tooth filling material includes, by mass, 15-35 parts of glycidyl methacrylate, 10-25 parts of Arabic gum, 5-20 parts of glass powder, 5-15 parts of silicon dioxide, 3-12 parts of nano montmorillonite, 1-6 parts of calcium carbonate, 0.5-3 parts of 1,6-hexanediol diacrylate, 0.8-3.5 parts of dicumyl peroxide, 0.3-1.5 parts of triethylene diamine, 0.2-1 part of EDTA, 0.2-1.2 parts of an organic tin stabilizer, 3-10 parts of zinc phosphate cement, and 0.1-0.5 parts of resorcinol monobenzoate. The tooth filling material has excellent mechanical performance and polishing performance, has the similar gloss and the similar coefficient of thermal expansion of a tooth, can effectively prevent edge micro-leakage and heat conductivity, has a good hole filling effect and is long in service life.

Description

technical field [0001] The invention relates to the technical field of dental materials, in particular to a tooth filling material and a preparation method thereof. Background technique [0002] In life, many people are facing dental problems, such as tooth decay, dental plaque, tooth fracture, etc. are common situations. Clinically, doctors often choose different materials to fill the cavity according to the location of the affected tooth, the location of the cavity, the magnitude of the occlusal force, as well as the patient's health and aesthetic requirements. Currently, the commonly used materials are: silver amalgam, composite Resin and glass ionomer complex. [0003] Composite resin materials are mainly composed of resin matrix and inorganic fillers. It has greater tensile strength and less expansion, shrinkage and deformation during curing. Its most prominent advantage is aesthetics, which can provide the best color matching with adjacent teeth. In the past, compos...

Claims

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Application Information

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IPC IPC(8): A61K6/097A61K6/02A61K6/027A61K6/898
CPCA61K6/831A61K6/836A61K6/898C08L5/00
Inventor 金仲恩全春兰张帆
Owner SUZHOU COSMETIC MATERIALS
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