Preparation method of low density and high strength foam glass sintering at low temperature

A foam glass and low-temperature sintering technology, applied in the field of multifunctional materials, can solve the problems of high foaming temperature, unsatisfactory porosity and mechanical properties, etc., and achieve the effects of high mechanical strength, simple and feasible process system, and fuel cost saving

Inactive Publication Date: 2016-09-21
TIANJIN UNIV
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  • Abstract
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  • Claims
  • Application Information

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Problems solved by technology

[0006] The purpose of the present invention is to overcome the deficiencies of the prior art that the foaming temperature is high, the porosity and the mechanical properties are not ideal enough, and provide a kind of mechanical properties such as low bulk density, relatively uniform pores, and compressive strength, and can A method for preparing cellular glass products that meet usage standards, are pure in color, and can be sintered at low temperature. In addition, firing cellular glass at a low temperature can not only reduce its production cost, but also greatly improve its production efficiency

Method used

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  • Preparation method of low density and high strength foam glass sintering at low temperature
  • Preparation method of low density and high strength foam glass sintering at low temperature
  • Preparation method of low density and high strength foam glass sintering at low temperature

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Embodiment 1

[0030] (1) Take 66g of silicon dioxide, 22.23g of sodium carbonate, 10.71g of calcium carbonate, 6g of aluminum oxide, 6.15g of magnesium carbonate, 4.4g of potassium carbonate, 1.41g of iron oxide, 1.29g of barium carbonate, and 1.06g of sodium sulfate with an electronic balance g, strontium oxide 0.05g. Add them together into the ball mill tank for dry grinding; the mass ratio of balls and materials is 2:1, and the mass ratio of large balls: medium balls: small balls is 1:2:1; ensure good sealing, and put them into high-temperature resistance furnace after dry grinding for 5 hours The temperature is raised to 1300°C to start melting, and the basic glass is obtained by water quenching immediately after being out of the furnace. Carry out ball milling with the same method after drying the broken basic glass obtained again, pass 140 mesh sieves after 5 hours and make basic glass powder.

[0031] (2) Take 60 g of basic glass powder and add 3.6 g of lithium carbonate into a ball...

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Abstract

The invention discloses a preparation method of low density and high strength foam glass sintering at low temperature. The glass powder is prepared from: by mass, SiO2 55.3-61.6%, Na2CO3 13.3-18.6%, CaCO3 9.0-11.6%, Al2O3 5-5.7%, MgCO3 3.56-5.8%, K2CO3 0.73-3.7%, Fe2O3 0.51-1.2%, BaCO3 0.53-1.1%, Na2SO4 0.47-0.9%, SrO 0.05-0.3%. The foam glass is prepared from glass powder, lithium carbonate using as a foaming agent 4-8 m%, and foam stabilizer 0-2 m% or foaming promoter 0-2 m%. The foam glass is prepared by sintering at low temperature of 725-775 DEG C and using a practical powder sintering method having convenient operation. The foam glass prepared by the invention has uniform pores, low density, and good mechanical properties, the properties such as porosity and water absorption can all reach the use standard, and the color is pure which is convenient to dye. In addition, the method can reduce the production cost, and can substantially improve the production efficiency.

Description

technical field [0001] The invention relates to a multifunctional material with light weight, high strength, heat preservation and sound insulation, in particular to a preparation method of low-temperature firing foam glass. Background technique [0002] Foam glass is an inorganic non-metallic foam material composed of a glass phase and a large number of uniform pores with a diameter of 0.5-5 mm. Foam glass has many excellent properties such as light weight and high strength, heat insulation and cold preservation, waterproof and anti-corrosion, non-toxic and non-combustible, chemical stability, insect resistance and bacteriostasis, ecological environmental protection, etc., making foam glass in many fields such as low temperature insulation, pipeline protection, noise reduction and noise reduction. has an irreplaceable role. But only a small amount of foam glass products are put into industrial production at present, and the output is also very limited. In the past, the ma...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03B19/08C03C12/00
CPCY02P40/57C03B19/08C03C12/00
Inventor 朱玉梅方馨悦
Owner TIANJIN UNIV
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