Method for extraction and derivatization of piperazine residues in tissue of fowls and pigs
A derivatization and piperazine technology, applied in the fields of solid phase extraction purification and acetic anhydride pre-column derivatization, can solve the problems of poor peak shape and tailing
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[0014] 1. Experiment with poultry and pig feeding and sample collection
[0015] Three-way cross-bred pigs and poultry were selected at the market age, namely, 16-week-old Jinghai yellow chicken, 10-week-old Yangzhou goose, 8-week-old cherry valley duck, and 6-month-old Du×long×big three-way crossbred pigs 6 The head, half male and half female, are raised in a single cage (column), fed with full feed without any drugs, and free drinking water. After 2 weeks of feeding, muscle, liver, kidney, skin and adipose tissue of the test animals were taken as blank tissue samples when they were slaughtered, and stored at -35°C. The samples were minced and homogenized during use.
[0016] 2. The extraction, purification and derivatization steps of the present invention
[0017] 1) Accurately weigh (2.0±0.02)g of a homogenized blank tissue sample, grind and mix with 3.0g anhydrous sodium sulfate in a mortar to absorb sample moisture;
[0018] 2) Add about 3.0g of diatomaceous earth and grind it t...
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