High-toughness ceramic nozzle material and preparation method thereof
A ceramic nozzle and high toughness technology, which is applied in the field of high toughness ceramic nozzle materials and its preparation, can solve the problems of insufficient toughness and short service life, and achieve the effects of improving deformation resistance, high density and increasing corrosion resistance
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Embodiment 1
[0024] A high-toughness ceramic nozzle material, consisting of the following raw materials in parts by weight: 70 parts of silicon nitride, 26 parts of boron nitride, 13 parts of nano-silicon carbide, 10 parts of magnesium fluoride, 18 parts of chromium carbide, and 15 parts of aluminum oxide , 13 parts of titanium diboride, 5 parts of kaolin, 3 parts of halloysite, 1 part of light calcium carbonate, 9 parts of magnesium oxide, 1 part of water glass, 5.3 parts of n-butyl acetate, 3.5 parts of carboxymethyl cellulose, 0.8 parts of lead naphthenate.
[0025] The preparation method of the high-toughness ceramic nozzle material described in this embodiment, the steps are as follows:
[0026] 1) Weigh magnesium fluoride, chromium carbide and kaolin, put them into a dry ball mill, and ball mill and mix for 2 hours to obtain the first mixed powder;
[0027] 2) Put the first mixed powder into a calciner, calcinate at 960°C for 1 hour, and quench in water to obtain a calcined material...
Embodiment 2
[0037] A high-toughness ceramic nozzle material, consisting of the following raw materials in parts by weight: 72 parts of silicon nitride, 32 parts of boron nitride, 15 parts of nano-silicon carbide, 14 parts of magnesium fluoride, 18 parts of chromium carbide, and 16 parts of aluminum oxide , 14 parts of titanium diboride, 8 parts of kaolin, 3 parts of halloysite, 2 parts of light calcium carbonate, 13 parts of magnesium oxide, 1 part of water glass, 5.5 parts of n-butyl acetate, 4.8 parts of carboxymethyl cellulose, 0.8 parts of lead naphthenate.
[0038] The preparation method of the high-toughness ceramic nozzle material described in this embodiment, the steps are as follows:
[0039] 1) Weigh magnesium fluoride, chromium carbide and kaolin, put them into a dry-process ball mill, and ball mill and mix for 3 hours to obtain the first mixed powder;
[0040] 2) Put the first mixed powder into a calciner, calcinate at 970°C for 2 hours, and quench in water to obtain a calcin...
Embodiment 3
[0050] A high-toughness ceramic nozzle material, which consists of the following raw materials in parts by weight: 72.5 parts of silicon nitride, 29 parts of boron nitride, 15 parts of nano-silicon carbide, 12 parts of magnesium fluoride, 20 parts of chromium carbide, and 17 parts of aluminum oxide , 15 parts of titanium diboride, 6.4 parts of kaolin, 4.7 parts of halloysite, 3 parts of light calcium carbonate, 11 parts of magnesium oxide, 1.8 parts of water glass, 5.7 parts of n-butyl acetate, 4.2 parts of carboxymethyl cellulose, 1.1 parts of lead naphthenate.
[0051] The preparation method of the high-toughness ceramic nozzle material described in this embodiment, the steps are as follows:
[0052] 1) Weigh magnesium fluoride, chromium carbide and kaolin, put them into a dry-process ball mill, and ball mill and mix for 2.5 hours to obtain the first mixed powder;
[0053] 2) Put the first mixed powder into the calciner, calcinate at 980°C for 1.5h, and quench in water to o...
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