Preparation method and application of magnetic hierarchical porous carbon material
A technology of multi-level pores and carbon materials, applied in chemical instruments and methods, other chemical processes, alkali metal oxides/hydroxides, etc., can solve the problems that single-pore structure carbon materials cannot meet high-performance applications, and achieve good Effect of magnetic separation performance and reproducibility, short process and stable performance
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Embodiment 1
[0026] Fully grind 4.0g of ferric nitrate and 20g of tripotassium ethylenediaminetetraacetic acid salt, take 15g of sample and simultaneously carbonize and activate it in a tube furnace at a temperature of 750°C and a heating rate of 3°C min -1 , maintained for 1.0 h; the obtained product was washed several times with a mixture of ethanol and distilled water, vacuum filtered, washed with water until neutral, and dried to obtain a magnetic hierarchical porous carbon material.
[0027] The static adsorption experiment was completed; 10mL of chloramphenicol solutions of different concentrations were added to the centrifuge tube, and 2.0mg of magnetic hierarchical porous carbon materials were added thereto, and left standing in a constant temperature water bath. The pH value of the solution, the amount of adsorbent, The impact of contact time and temperature on the adsorption of chloramphenicol; after the adsorption reaches saturation, the supernatant is collected by filtration wit...
Embodiment 2
[0037]Fully grind 2.0g ferric nitrate and 20g dipotassium ethylenediaminetetraacetic acid salt, take 15g sample and carbonize and activate it synchronously in a tube furnace at a temperature of 800°C and a heating rate of 5°C min -1 , maintained for 1.0 h; the obtained product was washed several times with a mixture of ethanol and distilled water, vacuum filtered, washed with water until neutral, and dried to obtain a magnetic hierarchical porous carbon material. According to the steps of Example 1, the resulting equilibrium adsorption capacity is 407.7mg g -1 . At an initial concentration of 300mg L -1 , when the temperature is 298K, the adsorption equilibrium is reached in about 400min.
Embodiment 3
[0039] Fully grind 1.0g ferric nitrate and 20g tripotassium ethylenediaminetetraacetic acid salt, take 15g samples and carbonize and activate them synchronously in a tube furnace at a temperature of 850°C and a heating rate of 10°C min -1 , maintained for 2.0 h; the obtained product was washed several times with a mixture of ethanol and distilled water, vacuum filtered, washed with water until neutral, and dried to obtain a magnetic hierarchical porous carbon material. Operated according to the steps of Example 1, the resulting equilibrium adsorption capacity is 444.2mg g -1 . At an initial concentration of 300mg L -1 , when the temperature is 298K, the adsorption equilibrium is reached in about 350min.
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