Method for preparing three-dimensional paper chip based on multi-edition patterning and silk screen combined printing technology
A printing technology, screen printing technology, applied in the direction of chemical instruments and methods, laboratory containers, laboratory utensils, etc., can solve the problems of complex production process, high cost, low precision, etc., and achieve simple equipment and improved The effect of precision and simplification of production steps
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[0038] Example 1
[0039] Select 300 mesh patterned printing ink screen, the material is nylon, the screen tension is 18N / cm, and use this patterned printing ink screen to make hydrophobic printing composed of 3:1 screen printing ink and ethyl acetate. Liquid, printed on filter paper, the screen distance between the ink screen and the filter paper during printing is 1.5mm, the contact angle of the scraper and the ink screen is 45°, the printing speed is 0.2m / s, the paper The pressure is 12N to obtain the channel layer and detection layer of the paper chip (2D paper chip).
[0040] The pretreatment agent uses a chemical masking agent, specifically sodium malonate with a mass ratio of 20% and 15% sodium fluoride. Use a mixed solution of EDTA and HF (EDTA: 0.05 mol l) as the color developing agent sodium diethyldithiocarbamate -1 ; HF: 0.05mol l -1 ) Configure to 1.0mg ml -1 Use 2% (v / v) ammonia water to adjust the pH to 8.5 to obtain the detection agent.
[0041] Select 400-mesh patt...
Example Embodiment
[0044] Example 2
[0045] Select 400 mesh patterned printing ink screen, the material is nylon, the screen tension is 18N / cm, and use this patterned printing ink screen to print a hydrophobic printing liquid composed of acrylic pigment and ethanol with a volume ratio of 1:1. On filter paper, the screen distance between the ink screen and the filter paper during printing is 1.5mm, the contact angle of the squeegee and the ink screen is 45°, the printing speed is 0.2m / s, and the pressure on the paper is 12N, obtain the channel layer and detection layer of the paper chip (2D paper chip).
[0046] The pretreatment agent uses a chemical masking agent, specifically Na 2 S 2 O 3 (40ppm) and 0.05%(v / v)H 2 SO 4 The mixed solution. Use 50% (v / v) acetone aqueous solution to make 2mg ml of color developer diacetyl oxime -1 Solution (the solution also contains EDTA: 0.05mol l -1 , Na 2 S 2 O 3 :0.05mol l -1 ), get the detection agent.
[0047] Select 400 mesh patterned drug printing screen, its...
Example Embodiment
[0050] Example 3
[0051] Select 200 mesh patterned printing ink screen, the material is nylon, the screen tension is 15N / cm, and the hydrophobic printing liquid composed of paraffin wax and n-heptane with a mass ratio of 1:150 is used for printing. On the cellulose acetate film, the screen distance between the ink screen and the cellulose acetate film during printing is 1.8mm, the angle when the squeegee is in contact with the ink screen is 40°, and the printing speed is 0.6m / s, the cellulose acetate membrane is subjected to a pressure of 4N to obtain the channel layer and detection layer of the paper chip (2D paper chip).
[0052] The pretreatment agent is ammonia water with a volume fraction of 2%, and the detection agent is diacetyl oxime with a concentration of 2 mg / ml.
[0053] Select 300-mesh patterned printing drug screen, its material is nylon, the screen tension is 15N / cm; use the patterned printing drug screen to print the above pretreatment agent on figure 1 As shown in...
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