Preparation method of anti-aging polypropylene fiber
A polypropylene fiber, anti-aging technology, applied in fiber chemical characteristics, rayon manufacturing, conjugated synthetic polymer rayon, etc., can solve the problems of poor thermal stability, easy ash absorption, airtight and other problems
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Embodiment 1
[0027] Embodiment 1: a kind of preparation method of antiaging polypropylene fiber, adopt following steps:
[0028] A) According to the number of parts by mass, take 0.8 parts of wollastonite needle-shaped fibers with an aspect ratio of 14:1, 0.5 parts of laurylamine polyoxyethylene ether, 0.6 parts of rutile titanium dioxide, and 0.2 parts of characteristic parameters with a diameter of 0.5 μm and a length of 5 μm aluminum borate whiskers, 0.3 parts of characterization parameters of 0.5 μm long, 0.01 μm wide concave-convex rod crystals, 4.0 parts of 20% sodium bicarbonate aqueous solution, 0.2 parts of nano-montmorillonite, mixed with superheated steam at 150 ° C Stir and steam in the reaction kettle for 45 minutes, irradiate with vacuum microwave at 300°C for 2h, then immerse in 80 parts of 30% sulfamic acid solution for vacuum moisture absorption treatment, heat to 60°C and ultrasonically disperse for 0.5h after absorption, and then Stir and disperse for 2 hours, take the s...
Embodiment 2
[0032] Embodiment 2: a kind of preparation method of antiaging polypropylene fiber, adopt following steps:
[0033] A) According to the number of parts by mass, 1.0 parts of wollastonite needle-like fibers with an aspect ratio of 15:1, 0.75 parts of laurylamine polyoxyethylene ether, 0.6 parts of rutile titanium dioxide, and 0.3 parts of characterization parameters have a diameter of 0.75 μm and a length of 15 μm of aluminum borate whisker, 0.4 parts of characterization parameter length of 2.5 μm, width of 0.05 μm concave-convex rod crystal, 5..0 parts of sodium bicarbonate aqueous solution with a mass fraction of 25%, 0.3 parts of nano-montmorillonite mixed, at 160 Stir and steam in a superheated steam reactor at ℃ for 50min, irradiate with vacuum microwave at 350℃ for 3h, then immerse in 100 parts of sulfamic acid solution with a mass fraction of 30% for vacuum moisture absorption treatment, heat to 75℃ after absorption and ultrasonically disperse for 1h , then stir and disp...
Embodiment 3
[0037] Embodiment 3: a kind of preparation method of antiaging polypropylene fiber, adopt following steps:
[0038] A) According to the number of parts by mass, take 1.2 parts of wollastonite needle-shaped fibers with an aspect ratio of 16:1, 1.0 parts of laurylamine polyoxyethylene ether, 1.0 parts of rutile titanium dioxide, and 0.4 parts of characterization parameters. The diameter is 1 μm and the length is 20 μm. Aluminum borate whiskers, 0.5 parts of characterization parameters are 5 μm long, 0.10 μm wide as concave-convex rod crystals, 6.0 parts of 30% sodium bicarbonate aqueous solution, 0.4 parts of nano-montmorillonite, mixed in a superheated steam reactor at 170 ° C Internal stirring and steaming reaction for 60min, vacuum microwave irradiation at 400°C for 4h, then immerse in 120 parts of 30% sulfamic acid solution for vacuum moisture absorption treatment, after absorption, heat to 95°C for ultrasonic dispersion for 1.5h, then stir to disperse 4h, take the suspensio...
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