A self-assembled catalyst coating filter material and preparation method thereof
A catalyst coating, catalyst technology, applied in chemical instruments and methods, separation methods, dispersed particle filtration, etc., can solve the problems of high treatment cost, large floor space, complex system, etc., to improve coverage and prolong service life , the effect of simple process
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Embodiment 1
[0043] A preparation method for a self-assembled catalyst coating filter material, comprising the steps of:
[0044] Prepare mixed solution a so that it contains 10g / L cationic polyelectrolyte (a mixed solution composed of polyallylamine hydrochloride and polyvinylamine in a volume ratio of 3:1), 10g / L triethylenetetramine, 0.1mol / Inorganic salt of L (mass ratio of sodium chloride and sodium sulfate 1:1); completely immerse the glass fiber filter material in the mixture a, deposit for 15 minutes; use water as solvent, prepare MnO with a mass fraction of 4% 2 / TiO 2 Catalyst dispersion, and fully stirred to disperse, the MnO 2 / TiO 2 The particle size of nanoparticles is 200nm; take out the glass fiber filter material from the mixture a, and dry it thoroughly in hot air at 70°C; immerse the dried glass fiber filter material in the dispersion liquid b, and let it stand for 15 minutes Thoroughly dry with hot air at 70°C; put the dried glass fiber filter into an oven, raise th...
Embodiment 2
[0046] A preparation method for a self-assembled catalyst coating filter material, comprising the steps of:
[0047] Prepare mixed solution a, make it comprise the anionic polyelectrolyte (polystyrene sulfonic acid) of 20g / L, the polyisocyanate of 5g / L, the inorganic salt (ammonium chloride) of 0.05mol / L; Completely submerge in the mixture a, let it stand for 15 minutes, take out the excess solution, and then dry it thoroughly in hot air at 80°C; prepare a Pt metal nanoparticle N-N dimethylformamide dispersion with a mass fraction of 6% , use a spray gun to evenly spray onto the surface of the dried polyphenylene sulfide filter material, make it fully wet, let it stand for 10 minutes, prick off the excess dispersion liquid, dry it with hot air at 80°C, bake at 160°C for 15 minutes, and take it out naturally Cool down. According to scanning electron microscope observation, there is a layer of Pt metal nanoparticles on the fiber surface of the polyphenylene sulfide filter mater...
Embodiment 3
[0049] A preparation method for a self-assembled catalyst coating filter material, comprising the steps of:
[0050] Prepare mixed solution a, make it comprise the cationic polyelectrolyte (polyethylene amine) of 15g / L, the N-methylolacrylamide of 10g / L, the inorganic salt (potassium chloride) of 0.15mol / L; The ethylene filter material is completely submerged in the mixed solution a, and deposited for 15 minutes; using water as a solvent, prepare V with a mass fraction of 3%. 2 o 5 / TiO 2 dispersion, and fully stirred evenly, the V 2 o 5 / TiO 2 The particle size of the catalyst nanoparticles is 100nm; the polytetrafluoroethylene filter material is taken out from the mixed liquid a, and thoroughly dried in hot air at 70°C; the dispersion liquid b is evenly sprayed onto the dried polytetrafluoroethylene filter material with a spray gun. until the PTFE filter material is completely soaked; after standing for 15 minutes, dry it thoroughly with hot air at 70°C; put the dried P...
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