Preparation method of ferrous saccharose complex

A technology of iron sucrose and complexes, which is applied in the field of complexes to achieve the effects of improving production efficiency, good solubility, and good stability

Active Publication Date: 2016-12-21
南宁市泽威尔饲料有限责任公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] There is no public report on the application of a single iron sucrose in feed additives

Method used

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  • Preparation method of ferrous saccharose complex
  • Preparation method of ferrous saccharose complex
  • Preparation method of ferrous saccharose complex

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] The preparation method of iron sucrose complex comprises the steps:

[0037] Step 1. Add 25 parts by weight of sucrose to the reaction kettle, add 40 parts by weight of water to dissolve the sucrose, add aqueous sodium hydroxide solution to alkalinize, and adjust the pH of the solution to 11;

[0038] Step 2: Heating the reaction kettle, keeping the temperature in the kettle at 65°C, and then adding 80 parts by weight of ferrous sulfate heptahydrate for complexation reaction for 1 hour, stirring continuously during the reaction process, generating iron sucrose solution, cooling, filtering and separating to obtain filter residue and filtrate ;

[0039] Step 3: According to the weight ratio of filtrate: 75% ethanol aqueous solution = 1:2, add 75% ethanol aqueous solution to precipitate at room temperature, the precipitation time is 1.5 hours, the precipitate is centrifugally filtered, and the obtained waste water is recycled, and the precipitate is vacuum-dried , detect ...

Embodiment 2

[0043] The preparation method of iron sucrose complex comprises the steps:

[0044] Step 1, add 29 parts by weight of sucrose to the reactor, add 45 parts by weight of water to dissolve the sucrose, add aqueous sodium hydroxide solution to alkalinize, and adjust the pH of the solution to 11 to obtain a reaction solution;

[0045] Step 2, heating the reaction kettle, keeping the temperature in the kettle at 70°C, and then adding 40 parts by weight of ferric chloride to carry out complexation reaction for 1.5 hours, stirring continuously during the reaction process, generating iron sucrose solution, cooling and filtering to separate, and obtaining filter residue and filtrate;

[0046] Step 3: According to the weight ratio of filtrate: 75% ethanol aqueous solution = 1:2, add 75% ethanol aqueous solution to carry out normal temperature precipitation, the precipitation time is 2 hours, the precipitate is subjected to centrifugal suction filtration, and the waste water obtained is re...

Embodiment 3

[0050] The preparation method of iron sucrose complex comprises the steps:

[0051] Step 1. Add 32 parts by weight of sucrose to the reaction kettle, add 50 parts by weight of water to dissolve the sucrose, and then alkalize the solution by adding aqueous sodium hydroxide solution to adjust the pH of the solution to 12;

[0052] Step 2, heating the reaction kettle, keeping the temperature in the kettle at 75° C., then adding 42 parts by weight of ferrous carbonate to carry out complexation reaction for 2 hours, stirring continuously during the reaction process, generating iron sucrose solution, cooling and filtering to separate, and obtaining filter residue and filtrate;

[0053] Step 3, take the filtrate obtained in step 2, according to the weight ratio of filtrate:75% ethanol aqueous solution=1:2, add 75% ethanol aqueous solution to carry out normal temperature precipitation, the precipitation time is 3 hours, the sediment is subjected to centrifugal suction filtration, and t...

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Abstract

The invention discloses a preparation method of a ferrous saccharose complex. The preparation method comprises the steps of obtaining a ferrous saccharose solution through complex reaction of saccharose and ferric salt; cooling and filtering to obtain filter residues and a filter liquor; adding ethanol water into the filter liquor to precipitate the complex; centrifugally pumping and filtering precipitates; vacuum drying to obtain a pure ferrous saccharose complex product; detecting ferric ion concentration of the filter residues; continuously adding the saccharose and ferrous salt according to the molar ratio of the saccharose to ferric ions being 1 to 4; returning the centrifugally pumped and filtered waste water into a reaction kettle so as to be used as a mother liquor for dissolving the saccharose, and carrying out circular reaction to continuously generating ferrous saccharose. According to the process for preparing the ferrous saccharose provided by the invention, the resource is not wasted, the production cost is reduced, and the production efficiency is improved. The obtained ferrous saccharose has the advantages of safety, high efficiency and high cost performance, and can be applied in production of an animal feed with comprehensive nutrition.

Description

technical field [0001] The invention relates to a complex, especially a sucrose iron complex and a preparation method thereof, and discloses the use thereof. Background technique [0002] Nutritional and physiological functions of iron: 1. As a carrier and enzyme component: iron participates in the composition of hemoglobin and myoglobin, and is responsible for the important role of oxygen and carbon dioxide in the carrier. In addition, iron is directly involved in the composition of cytochrome oxidase, peroxidase and xanthine oxidase. Divalent or ferric iron ions are indispensable activating factors for various enzymes that activate carbohydrate metabolism; 2. Participate in protein synthesis and energy metabolism: the content of iron in animals directly affects the content of phosphorus. The synthesis of DNA will be inhibited due to phosphorus deficiency, and the mitochondria and microsomes in tissue cells will be abnormal. In addition, iron, as a component of cytochrome...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07H1/00C07H23/00A23K20/20A23K20/163
CPCC07H1/00C07H23/00
Inventor 周建群
Owner 南宁市泽威尔饲料有限责任公司
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