Attapulgite modification based PP (polypropylene) melt-blown filter cartridge and preparation method thereof
The technology of melt-blown filter element and attapulgite is applied in the field of PP melt-blown filter element modified based on attapulgite and its preparation, which can solve the problems of restricting the development of PP filter element, filtering liquid pollution, breeding microorganisms, etc.
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[0017] The invention provides a method for preparing a PP melt-blown filter element modified based on attapulgite, comprising:
[0018] 1) spraying the polymer coating on the surface of attapulgite, then drying, soaking in dilute sulfuric acid solution, and filtering to obtain activated attapulgite;
[0019] 2) spray silver nitrate solution and hydrazine sulfate solution on the surface of activated attapulgite at the same time, and let it stand to prepare silver-modified attapulgite;
[0020] 3) decocting and filtering the Chinese herbal medicine in water to obtain the Chinese herbal medicine extract and the Chinese herbal medicine filter cake;
[0021] 4) In the presence of protective gas, place the silver-modified attapulgite at 240-255°C for calcination for 25-40 minutes, then place the calcined product in Chinese herbal medicine extract for impregnation and filtration to obtain Chinese herbal medicine-modified attapulgite earth;
[0022] 5) PP (polypropylene), AES (acryl...
Embodiment 1
[0041] 1) Polymer coating (containing polyvinyl alcohol, 1.2% by weight of p-aminophenol platinum, 0.7% by weight of palladium (II)-2-(5-bromo-2-pyridylazo)-5-diethylaminophenol ) sprayed on the surface of attapulgite, then dried at 125°C for 6h, soaked in 50°C and 18% by weight dilute sulfuric acid solution for 2h, and filtered to obtain activated attapulgite, wherein attapulgite, polymer The weight ratio of paint and dilute sulfuric acid solution is 100:4:200;
[0042] 2) Spray 5% by weight of silver nitrate solution and 2.5% by weight of hydrazine sulfate solution on the surface of activated attapulgite at the same time, and let it stand at 30° C. for 5 hours to obtain silver-modified attapulgite, wherein activated attapulgite, The weight ratio of silver nitrate solution and hydrazine sulfate solution is 100:7:11;
[0043] 3) Mix lemongrass, scallion, licorice, mulberry leaves, forsythia, golden boil grass, red peony, red euphorbia, Magnolia officinalis and water according...
Embodiment 2
[0047] 1) Polymer coating (containing polyvinyl alcohol, 0.8% by weight of p-aminophenol platinum, 0.2% by weight of palladium (II)-2-(5-bromo-2-pyridylazo)-5-diethylaminophenol ) sprayed on the surface of attapulgite, then dried at 120°C for 5h, placed in 45°C and 15% by weight of dilute sulfuric acid solution for 1h soaking, and filtered to obtain activated attapulgite, wherein attapulgite, polymer The weight ratio of paint and dilute sulfuric acid solution is 100:3:150;
[0048] 2) Spray 4% by weight of silver nitrate solution and 2% by weight of hydrazine sulfate solution on the surface of activated attapulgite at the same time, and let it stand at 25° C. for 4 hours to obtain silver-modified attapulgite, wherein activated attapulgite, The weight ratio of silver nitrate solution and hydrazine sulfate solution is 100:5:10;
[0049] 3) Mix lemongrass, scallion, licorice, mulberry leaves, forsythia, golden boiling grass, red peony, red euphorbia, magnolia officinalis and wat...
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