A kind of preparation method of antibacterial PVC polyester covering silk
A technology of covering silk and antioxidants, which is applied in the chemical post-processing of synthetic polymer rayon, yarn, textiles and paper making, etc. Stiff hand, good antibacterial effect
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[0027] The invention discloses a preparation method of antibacterial PVC polyester coated yarn, which mainly comprises two steps of preparing a masterbatch and coating the masterbatch with polyester yarn.
[0028] The preparation of color masterbatch comprises the following steps:
[0029] a, in parts by mass, weigh each component raw material;
[0030] b. Put the raw materials of each component into the high-speed mixer for high-speed mixing;
[0031] c. After stirring and cooling to 50 degrees, transfer to the hopper, and the hopper is sent into the main engine hopper through the conveying device;
[0032] d. Cut into particles by a granulator, that is, masterbatch.
[0033] The speed of high-speed mixing is 700-800 rpm.
[0034] The steps of polyester filament coating masterbatch are:
[0035] a. The filaments are put into the filament frame, passed through the tensioner positioning device into the mold, and the mold is loaded into the shunt
[0036] b. Put the masterb...
Embodiment 1
[0054] A kind of preparation method of antibacterial PVC polyester covering silk, comprises the following steps:
[0055] 1) Preparation of color masterbatch
[0056] a. In parts by mass, weigh the raw materials of the following components
[0057] 69 parts of polyvinyl chloride, 6 parts of pigment, 8 parts of dispersant, 4 parts of antioxidant, 5 parts of flame retardant, 8 parts of nano-zinc oxide surface grafted powder;
[0058] b. Put the raw materials of each component into the high-speed mixer for high-speed mixing;
[0059] c. After stirring and cooling to 50 degrees, transfer to the hopper, and the hopper is sent into the main engine hopper through the conveying device;
[0060] d. Cut into particles by a granulator, that is, masterbatch;
[0061] 2), coating
[0062] a. The filaments are put into the filament frame, passed through the tensioner positioning device into the mold, and the mold is loaded into the shunt
[0063] b. Put the masterbatch into the hopper,...
Embodiment 2
[0067] Preparation of nano zinc oxide surface graft powder:
[0068] a. Take 3 parts of silane coupling agent KH-570, 4 parts of tridecafluorooctyltrimethoxysilane, add 120 parts of ethanol; water = 4:1 aqueous solution of absolute ethanol, hydrolyze at room temperature for 1 hour; Add 14 parts of nano-zinc oxide dried at 120°C for 12 hours, add 30 parts of ethanol; water = 4:1 aqueous solution of absolute ethanol, ultrasonically disperse for 30 minutes; then mix the two into a flask, heat up to 80°C while stirring, and react for 12 hours After the reaction is finished, cool to room temperature, centrifuge the reactant at 4000r / min for 20min, and wash repeatedly with absolute ethanol to remove unreacted coupling agent; put it into a desiccator after fully drying in a vacuum oven to obtain surface-modified nano Zinc oxide white powder;
[0069] b. Take 10 parts of surface-modified nano-zinc oxide powder, add 84 parts of absolute ethanol, and ultrasonically disperse for 30 minu...
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