Insecticidal composition containing clothianidin, chlopyrifos and chlorantraniliprole, and preparation method thereof
A kind of technology of chlorantraniliprole and insecticidal composition, applied in the field containing clothianidin
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Embodiment 1
[0055] A clothianidin containing. Chlorpyrifos. The insecticidal composition of chlorantraniliprole, which is made from the raw materials of the following mass fractions:
[0056]
[0057] The above-mentioned clothianidin. Chlorpyrifos. The preparation method of the insecticidal composition preparation of chlorantraniliprole, the steps are:
[0058] A. According to the designed formula, weigh clothianidin, chlorpyrifos, and chlorantraniliprole, and put them into a container, then add sodium lauryl sulfate, Morwet EFW, and sodium lignosulfonate Salt, MorwetD-425, ethylene glycol, sodium carboxymethylcellulose, white carbon black, stir well;
[0059] B. Stir at high speed (1000 rpm) to pre-disperse for 25-35 minutes, then stop stirring (to achieve complete homogeneity), add sanding medium, and start sanding;
[0060] C. Stop sanding after 1.8-2.2h (to 98% of the suspended particle size is between 0.1-0.7μm), filter, remove the glass beads, add other additives (AF9903, so...
Embodiment 2
[0062] A clothianidin containing. Chlorpyrifos. The effervescent tablet of the insecticidal composition of chlorantraniliprole, it is made of the raw material of following mass fraction:
[0063]
[0064] The above-mentioned clothianidin. Chlorpyrifos. The preparation method of the insecticidal composition preparation of chlorantraniliprole, the steps are:
[0065] A. According to the designed formula, weigh clothianidin. Chlorpyrifos. Chlorantraniliprole technical, put into a holding container, then add sodium lauryl sulfate and Morwet EFW, sodium lignosulfonate and GY-W04, citric acid and starch, white carbon black and diatomaceous earth sample, mixed homogeneously to obtain a mixture;
[0066] B, the mixture is pulverized on a high-energy pulverizer for 8-12min (200 mesh), and then pulverized in a jet pulverizer (200 mesh) to make 40% powder;
[0067] C. Add the powder to an aqueous binder (dextrin) solution, stir evenly, dry, and tablet to obtain effervescent tab...
Embodiment 3
[0069] A clothianidin containing. Chlorpyrifos. Chlorantraniliprole insecticidal composition tank mix preparation method and tank mix technology thereof,
[0070]
[0071]The above-mentioned clothianidin. Chlorpyrifos. A preparation method and a mixing method of an insecticidal composition tank mix of chlorantraniliprole, the steps of which are:
[0072] A. According to the experimental design, make clothianidin into one of water-dispersible granules, suspension concentrates, wettable powders, and emulsifiable concentrates; make chlorpyrifos into one of emulsifiable concentrates, wettable powders, microemulsions, and water-emulsions ; Chlorantraniliprole is made into one of suspension concentrate, water dispersible granule, emulsifiable concentrate, and wettable powder.
[0073] B. Weigh 20% clothianidin suspending agent according to the calculated dosage, add 1000-2000ml of water, stir and dissolve;
[0074] C. After 20% clothianidin suspending agent is dissolved, add...
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