Preparation method of epitaxially-growing silicon carbide-graphene film
A graphene film, epitaxial growth technology, applied in chemical instruments and methods, crystal growth, single crystal growth and other directions, can solve problems such as lattice defects on the surface of SiC substrates, deposition of silicon compounds, reduction of silicon enrichment on the surface of SiC, etc. Achieve the effect of reducing lattice defects and serious reduction of surface silicon enrichment, and good crystal quality
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[0017] The preparation method of epitaxial growth silicon carbide-graphene film, comprises the steps:
[0018] (1) Preparation of silicon carbide-graphene
[0019] Carry out cleaning pretreatment on the silicon carbide substrate. After the cleaning is completed, directly put the SiC substrate silicon side up and put it into the equipment to prepare for epitaxial growth.
[0020] (2) Epitaxial growth of silicon carbide-graphene film
[0021] The first step is to carry out the homoepitaxial growth of 4H-SiC first: reduce the vacuum degree of the chamber to 8×10 -4 Below Pa, continuously feed 7L / min of H 2 , gradually increase the chamber temperature from room temperature to 1600°C; keep at 1600°C for 10min as a pre-growth stage, and then feed 9~15mL / min of SiH 4 and 2~6mL / min of C 3 h 8 After growing for 60 minutes, the scratches and defects on the surface of the substrate were filled and covered to form a new SiC surface with excellent performance; finally, the temperature...
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