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A kind of silver-loaded nano-titanium dioxide bactericidal anti-mildew diatom mud and preparation method thereof

A nano-titanium dioxide and diatom mud technology, applied in the field of diatom mud coatings, can solve the problems of reduced utilization rate of nano-materials, difficult to achieve bactericidal effect, small color selection range, etc., to improve uniformity, improve indoor air purification efficiency, The effect of improving the surface sterilization and mildew resistance

Inactive Publication Date: 2018-11-23
ZHONGSHAN BORUI BUILDING MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, it is difficult to disperse evenly when silver-loaded nanomaterials are directly added to powdered diatom mud, resulting in a greatly reduced utilization rate of the added nanomaterials, unable to exert their true efficiency, and difficult to achieve a satisfactory bactericidal effect
Powder diatom mud also has disadvantages such as dust pollution caused by on-site mixing, small range of color choices, finished products after mixing cannot be stored, and are easy to harden and deteriorate.

Method used

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  • A kind of silver-loaded nano-titanium dioxide bactericidal anti-mildew diatom mud and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Add 17.5wt% deionized water to the reactor, add 0.2wt% dispersant, 0.1wt% wetting agent, 0.2wt% defoamer, 1wt% hydroxyethyl cellulose in sequence at 300 rpm, and disperse for 10 minutes , add 1wt% silver-loaded nano-titanium dioxide at a speed of 1500 rpm, and disperse at a high speed for 30 minutes until the fineness is below 50 μm to obtain a silver-loaded nano-titanium dioxide pre-pulp;

[0031] Add 22.3wt% deionized water to the reactor, add 1wt% glycerin, 2wt% nano-silica solution, 0.6wt% hydroxyethyl cellulose, and 0.3wt% bentonite in sequence at 300 rpm, and disperse for 15 minutes Finally, adjust the rotating speed to 1500 rpm, add 20wt% silver-loaded nano-titanium dioxide prefabricated slurry, 8wt% titanium dioxide, 15wt% 800 mesh ash calcium, 30wt% diatomite, 0.5wt% retarder, 0.3wt% ash Calcium stabilizer, stir and disperse evenly to get the finished product.

Embodiment 2

[0033] Add 19.4wt% deionized water to the reactor, add 0.2wt% dispersant, 0.1wt% wetting agent, 0.2wt% defoamer, 0.8wt% hydroxyethyl cellulose in sequence at 300 rpm, and disperse After 10 minutes, adjust the rotation speed to 1500 rpm and add 1.5wt% silver-loaded nano-titanium dioxide, and disperse at a high speed for 30 minutes until the fineness is below 50 μm to obtain a silver-loaded nano-titanium dioxide pre-pulp;

[0034] 29.7wt% deionized water was added to the reaction kettle, and 0.8wt% glycerol, 2.5wt% nano-silica solution, 0.3wt% hydroxyethyl cellulose, and 0.6wt% bentonite were added successively at 300 rpm. After dispersing for 15 minutes, adjust the speed to 1500 rpm, add 22.2wt% silver-loaded nano-titanium dioxide prefabricated slurry, 3wt% titanium dioxide, 12wt% 800 mesh ash calcium, 28wt% diatomaceous earth, 0.6wt% retarder, 0.3 Wt% ash calcium stabilizer, stir and disperse evenly to get the finished product.

Embodiment 3

[0036] Add 21.9wt% deionized water to the reactor, add 0.2wt% dispersant, 0.1wt% wetting agent, 0.2wt% defoamer, 0.6wt% hydroxyethyl cellulose in sequence at 300 rpm, and disperse After 10 minutes, adjust the rotation speed to 1500 rpm and add 2wt% silver-loaded nano-titanium dioxide, and disperse at a high speed for 30 minutes until the fineness is below 50 μm to obtain a silver-loaded nano-titanium dioxide pre-pulp;

[0037] Add 22wt% deionized water to the reaction kettle, add 1.2wt% glycerin, 3wt% nano-silica solution, 0.5wt% hydroxyethyl cellulose, 0.5wt% bentonite in sequence at 300 rpm, and disperse for 15 minutes Finally, adjust the rotating speed to 1500 rpm, add 25wt% silver-loaded nano-titanium dioxide prefabricated slurry, 5wt% titanium dioxide, 10wt% 800 mesh ash calcium, 32wt% diatomite, 0.5wt% retarder, 0.3wt% ash Calcium stabilizer, stir and disperse evenly to get the finished product.

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Abstract

The invention belongs to the field of diatom mud paint, and discloses silver-loaded nano titanium dioxide anti-mildew diatom mud and a preparation method thereof. The method is in particular as follows: first, silver-loaded nano titanium dioxide is made into 10-30wt% of prefabricated slurry, and the diatom mud is prepared from the 10-30wt% of prefabricated slurry, 20-35wt% of deionized water, 0.8-3wt% of an antifreezer, 2-5wt% of a nano silicon oxide solution, 0.2-1.0wt% of a thickening agent, 0.5-3wt% of bentonite, 3-15wt% of titanium dioxide, 5-20wt% of ash calcium, 25-40wt% of diatomite, 0.1-0.8wt% of a retarder and 0.1-2wt% of an ash calcium stabilizer. A coating which is obtained by forming a film from the diatom mud can capture oxygen free radicals decomposed from rotten substances and alkane molecules producing other peculiar smell, has a very strong killing effect on a variety of bacteria, and is anti-microbial and anti-mildew, the diatom mud needs no on-site mixing, product uniformity is improved, and dust pollution to the environment caused by on-site construction mixing can be avoided; a silver-loaded nano material has high surface activity, and is composited with the diatomite with physical adsorption effect, and surface anti-microbial and anti-mildew capability and indoor air purification efficiency of the diatom mud can be significantly improved.

Description

technical field [0001] The invention belongs to the field of diatom mud coatings, in particular to a silver-loaded nano-titanium dioxide sterilizing and anti-mold diatom mud and a preparation method thereof. Background technique [0002] As an indoor coating, diatom mud is favored by people because its construction, smearing and pattern making are superior to existing decorative coatings, it has super adsorption capacity, and it can also absorb harmful gases in the air. wide. [0003] Now the main component of diatom mud on the market is diatomite compounded with fillers, additives, binders, etc. The finished product is in the form of powder, which has a certain effect of adsorbing harmful gases, but the surface of the product has no Sterilization and purification function, directly adding silver-loaded nanomaterials to powder products can increase its sterilization and purification functionality, because nanomaterials have small particle size, increased specific surface ar...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B28/00C04B14/30C04B14/34C04B14/08
CPCC04B28/00C04B2111/00017C04B2103/408C04B2103/50C04B2103/0068C04B24/383C04B14/305C04B14/34C04B24/02C04B14/06C04B14/104C04B14/08C04B2103/22
Inventor 李军华张朝平钟顺玉
Owner ZHONGSHAN BORUI BUILDING MATERIAL CO LTD
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