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Tobacco natural plant dye, preparation method, and application thereof

A technology for natural plant dyes and tobacco, applied in the field of tobacco natural plant dyes and their preparation, can solve problems such as no reports, and achieve the effects of good market prospects, high color fastness to rubbing, and improvement of body immunity

Inactive Publication Date: 2017-04-26
广东印象派服装有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It can be seen from the above prior art that the pigments in tobacco and its tobacco products can be extracted by using various extraction methods. The pigments extracted from tobacco are mostly used to regulate the color of tobacco, but regarding the application of tobacco in natural plant dyes and dyeing research, no reports

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0041] (1) Wash 8g of fresh undried mature tobacco with amino acid-based surfactant to clean the impurities and dirt on the surface of the tobacco leaf, dry it, pulverize it with a pulverizer to form a 25-50 μm tobacco powder, and soak the tobacco powder in a pH value Soak in 8-9 enzyme-containing emulsion at 80-90°C for 150-180 minutes to remove part of the sugar and gum in the tobacco, take out, wash, filter and dry to obtain biologically pretreated tobacco powder.

[0042] (2) With the material-liquid ratio of 1g:80mL, add the biologically pretreated tobacco powder into the aqueous solution, soak for 2 hours for pretreatment, then add sodium bicarbonate to adjust the pH to 8, raise the temperature to 80°C, keep it warm for 180min, and filter to obtain Primary extract and filter residue.

[0043] (3) With the ratio of solid to liquid 1g:70mL, add the filter residue into the aqueous solution, soak for 2 hours for pretreatment, then add sodium bicarbonate to adjust the pH to 9...

Embodiment 2

[0048] (1) Wash 8g of fresh undried mature tobacco with amino acid-based surfactant to clean the impurities and dirt on the surface of the tobacco leaf, dry it in the air, pulverize it with a pulverizer to form 0.5-1 μm tobacco powder, and soak the tobacco powder in pH value Soak in 8-9 enzyme-containing emulsion at 80°C-90°C for 150-180min, remove part of the sugar and gum in the tobacco, take out, wash, filter and dry to obtain biologically pretreated tobacco powder.

[0049] (2) With a solid-liquid ratio of 1g:70mL, add the biologically pretreated tobacco powder into an aqueous solution or an ethanol aqueous solution with a volume ratio of 50%-75%, soak for 2 hours, and then add ethylenediamine to adjust the pH to 8 , heated up to 90°C, kept warm for 170min, and filtered to obtain primary extract and filter residue.

[0050] (3) With the ratio of solid to liquid 1g:70mL, add the filter residue into the aqueous solution, soak for 2 hours for pretreatment, then add sodium bic...

Embodiment 3

[0055] (1) Wash 8g of fresh undried mature tobacco with amino acid-based surfactant to clean the impurities and dirt on the surface of the tobacco leaf, dry it, pulverize it with a pulverizer to form a 25-50 μm tobacco powder, and soak the tobacco powder in a pH value Soak in 8-9 enzyme-containing emulsion at 80°C-90°C for 150-180min, remove part of the sugar and gum in the tobacco, take out, wash, filter and dry to obtain biologically pretreated tobacco powder.

[0056] (2) With a solid-liquid ratio of 1g:70mL, add the biologically pretreated tobacco powder into an aqueous ethanol solution with an ethanol content of 50%, soak for 2 hours, then add ethylenediamine to adjust the pH to 9, and heat up to 85°C , keep warm for 160min, and filter to obtain primary extract and filter residue.

[0057] (3) With the material-liquid ratio of 1g:80mL, add the filter residue to an ethanol aqueous solution with an ethanol content of 50%, soak for 2 hours, then add ethylenediamine to adjust...

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PUM

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Abstract

The invention provides a tobacco natural plant dye, a preparation method, and an application thereof. The tobacco natural plant dye is prepared from fresh tobacco as a raw material, which is washed with a surfactant and is subjected to bio-pretreatment impurity removal to obtain tobacco powder. The tobacco powder is extracted by a water solution or an ethanol water solution, wherein the pH value of the solution is controlled by NaHCO3 or ethylenediamine; the solution is subjected to heating extraction and is filtered to produce a natural dye stock liquid, which is concentrated, solidified and crushed to obtain the tobacco natural plant dye. In the method, tobacco pigments are used as natural dyes in the dyeing and finishing industry. The preparation method is simple and is high-effective. The tobacco natural plant dye can dye cotton, wool, cashmere and the like. Through regulation on a direct dyeing process, a pre-mordant dyeing process or a same-mordant dyeing process and types of mordants, fabrics in brown color, yellow-brown color, light-brown color, yellow color or green color can be produced. The dyed fabric has high color fastness to rubbing, has natural and gentle gloss and significantly improves usage value of tobacco and application value of the fabrics.

Description

technical field [0001] The invention belongs to the technical field of textile materials, in particular relates to natural dyes and their production and application, in particular to a tobacco natural plant dye and its preparation method and application. Background technique [0002] With the irreversible consumption of earth's oil resources and serious environmental pollution, under the influence of the global green wave, people are paying more and more attention to environmental and health issues, and some synthetic dyes have more and more negative effects on human health and the ecological environment. More attention has been paid to it. There are more than 20 kinds of carcinogenic aromatic amines, more than 100 synthetic dyes that may produce carcinogens, and dozens of dyes that are allergic to the skin. Therefore, it is imperative to develop natural and environmentally friendly dyes and environmentally friendly and clean dyeing processes. Natural environmental protectio...

Claims

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Application Information

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IPC IPC(8): C09B61/00D06P1/34D06P3/14D06P3/60D06P1/44
CPCC09B61/00D06P1/34D06P1/445D06P3/14D06P3/60
Inventor 李胜利张朝清
Owner 广东印象派服装有限公司
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