A kind of preparation method of n-doped carbon quantum dots and its products and applications
A technology of carbon quantum dots, which is applied in the field of preparation of N-doped carbon quantum dots, can solve the problems that carbon dots are in the preliminary stage, and achieve the effects of good water solubility, improved efficiency and high yield
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0039] Preparation of N-doped carbon quantum dots:
[0040] Step 1, weigh 0.5g of chitosan (degree of deacetylation is 90%, viscosity is 400mPa s) powder and place it in a clean 50mL beaker, add 25mL of deionized water, and stir at 600rpm at 20°C 20min.
[0041] Step 2, transfer the colorless solution to a polytetrafluoroethylene hydrothermal reaction kettle, place it in a vacuum drying oven, and heat at a constant temperature of 200° C. for 10 h.
[0042] Step 3, after the reaction is completed, the product to be synthesized is naturally cooled to 20°C.
[0043] Step 4, the obtained yellow solution is placed in a centrifuge and centrifuged at a speed of 12000r / min for 10min, and then filtered with a 0.22μm microporous filter head to obtain a clarified carbon quantum dot solution.
[0044] Step 5, vacuum freeze-dry the obtained clear carbon quantum dot solution at a temperature of -50° C. for 24 hours and a vacuum of 9.6 Pa to obtain N-doped fluorescent carbon quantum dot po...
Embodiment 2
[0052] Preparation of N-doped carbon quantum dots:
[0053] Step 1, weigh 0.5g of chitosan (degree of deacetylation is 95%, viscosity is 50mPa s) is placed in a clean 50mL beaker, add 25mL of deionized water, and stir at 400rpm for 30min at 25°C , a colorless and transparent aqueous solution was obtained.
[0054] Step 2: Transfer the colorless solution to a polytetrafluoroethylene hydrothermal reaction kettle, place in a vacuum drying oven, and heat at a constant temperature of 200° C. for 8 hours.
[0055] Step 3, after the reaction is completed, the product to be synthesized is naturally cooled to 10°C.
[0056] Step 4, the obtained yellow solution is placed in a centrifuge and centrifuged at a speed of 12000r / min for 10min, and then filtered with a 0.22μm microporous filter head to obtain a clarified carbon quantum dot solution.
[0057] Step 5, the obtained clear carbon quantum dot solution is vacuum freeze-dried at -50°C for 24 hours and the vacuum degree is 9.6Pa to o...
Embodiment 3
[0060] Preparation of N-doped carbon quantum dots:
[0061] Step 1, weigh 0.5g of chitosan (degree of deacetylation is 90%, viscosity is 800mPa·s) is placed in a 50mL clean beaker, add 30mL of deionized water, and stir at 500rpm for 20min at 10°C , a colorless and transparent aqueous solution was obtained.
[0062] Step 2, transfer the colorless solution to a polytetrafluoroethylene hydrothermal reaction kettle, place in a vacuum drying oven, and heat at a constant temperature of 190°C for 12h.
[0063] Step 3, after the reaction is completed, the product to be synthesized is naturally cooled to 20°C.
[0064] Step 4, the obtained yellow solution is placed in a centrifuge and centrifuged at a speed of 12000r / min for 10min, and then filtered with a 0.22μm microporous filter head to obtain a clarified carbon quantum dot solution.
[0065] Step 5, vacuum freeze-dry the obtained clear carbon quantum dot solution at a temperature of -54°C for 24 hours and a vacuum of 9.6 Pa to ob...
PUM
Property | Measurement | Unit |
---|---|---|
viscosity | aaaaa | aaaaa |
particle size | aaaaa | aaaaa |
particle size | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com