Antibacterial nanofibers or master batches
A technology of nanofibers and antibacterial fibers, which is applied in fiber processing, conjugated synthetic polymer artificial filaments, filament/thread forming, etc., can solve the problems of poor resistance to rubbing and pollution resistance, poor mechanical properties, etc., and achieve antibacterial Performance, thermal stability improvement, water solubility enhancement effect
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Embodiment 1
[0039] First, an antimicrobial polymer resin solution is prepared.
[0040] Taking mass as the unit, dissolve 1wt% photosensitive molecule (model YG-03, the manufacturer is Qingdao Sunshine Biomedical Technology Co., Ltd.) into 10wt% formic acid (mass fraction ≥88%) solution, and the average molecular weight is 50,000 of 6wt% polymer resin was dissolved into 60wt% dimethylacetamide, slowly heated to 60-80°C at a heating rate of 2-5°C per minute, stirred for 60-120 minutes to fully dissolve the polyurethane, add 0.01 wt % additive and fully stirred to obtain an antibacterial polyurethane electrospinning solution.
[0041] Next, the antibacterial polyurethane electrospinning solution was electrospun at a spinning speed of 12 ml / h and a voltage of 15 kV.
[0042] Finally, the obtained electrospinning fibers are dried at a temperature of 60° C. for 0.1-4 hours to remove the residual organic solvent to prepare antibacterial nanofibers.
Embodiment 2
[0044] First, an antimicrobial polymer resin solution is prepared.
[0045] Taking mass as the unit, dissolve 5wt% photosensitive molecule (model YG-01, the manufacturer is Qingdao Sunshine Biomedical Technology Co., Ltd.) into 10wt% formic acid (mass fraction ≥88%) solution, and the average molecular weight is 50,000 of 6wt% polymer resin was dissolved into 60wt% dimethylacetamide, slowly heated to 60-80°C at a heating rate of 2-5°C per minute, stirred for 60-120 minutes to fully dissolve the polyurethane, add 0.01 wt % additive and fully stirred to obtain an antibacterial polyurethane electrospinning solution.
[0046] Next, the antibacterial polyurethane electrospinning solution was electrospun at a spinning speed of 12 ml / h and a voltage of 15 kV.
[0047] Finally, the obtained electrospinning fibers are dried at a temperature of 60° C. for 0.1-4 hours to remove the residual organic solvent to prepare antibacterial nanofibers.
Embodiment 3
[0049] First, an antimicrobial polymer resin solution is prepared.
[0050] Taking mass as the unit, dissolve 10wt% photosensitive molecule (model YG-03, the manufacturer is Qingdao Sunshine Biomedical Technology Co., Ltd.) into 10wt% formic acid (mass fraction ≥88%) solution, and the average molecular weight is 50,000 of 6wt% polymer resin was dissolved into 60wt% dimethylacetamide, slowly heated to 60-80°C at a heating rate of 2-5°C per minute, stirred for 60-120 minutes to fully dissolve the polyurethane, add 0.01 wt % additive and fully stirred to obtain an antibacterial polyurethane electrospinning solution.
[0051] Next, the antibacterial polyurethane electrospinning solution was electrospun at a spinning speed of 12 ml / h and a voltage of 15 kV.
[0052] Finally, the obtained electrospinning fibers are dried at a temperature of 60° C. for 0.1-4 hours to remove the residual organic solvent to prepare antibacterial nanofibers.
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