Antibacterial nanofibers or master batches

A technology of nanofibers and antibacterial fibers, which is applied in fiber processing, conjugated synthetic polymer artificial filaments, filament/thread forming, etc., can solve the problems of poor resistance to rubbing and pollution resistance, poor mechanical properties, etc., and achieve antibacterial Performance, thermal stability improvement, water solubility enhancement effect

Inactive Publication Date: 2017-06-23
SUNDYNAMIC TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] The second purpose of the present invention is to enhance the antibacterial performance of existing nanofibers and masterbatches, overcome the shortcomings of their antibacterial materials and fabrics, plastics and other products with poor me

Method used

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  • Antibacterial nanofibers or master batches
  • Antibacterial nanofibers or master batches
  • Antibacterial nanofibers or master batches

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] First, an antimicrobial polymer resin solution is prepared.

[0040] Taking mass as the unit, dissolve 1wt% photosensitive molecule (model YG-03, the manufacturer is Qingdao Sunshine Biomedical Technology Co., Ltd.) into 10wt% formic acid (mass fraction ≥88%) solution, and the average molecular weight is 50,000 of 6wt% polymer resin was dissolved into 60wt% dimethylacetamide, slowly heated to 60-80°C at a heating rate of 2-5°C per minute, stirred for 60-120 minutes to fully dissolve the polyurethane, add 0.01 wt % additive and fully stirred to obtain an antibacterial polyurethane electrospinning solution.

[0041] Next, the antibacterial polyurethane electrospinning solution was electrospun at a spinning speed of 12 ml / h and a voltage of 15 kV.

[0042] Finally, the obtained electrospinning fibers are dried at a temperature of 60° C. for 0.1-4 hours to remove the residual organic solvent to prepare antibacterial nanofibers.

Embodiment 2

[0044] First, an antimicrobial polymer resin solution is prepared.

[0045] Taking mass as the unit, dissolve 5wt% photosensitive molecule (model YG-01, the manufacturer is Qingdao Sunshine Biomedical Technology Co., Ltd.) into 10wt% formic acid (mass fraction ≥88%) solution, and the average molecular weight is 50,000 of 6wt% polymer resin was dissolved into 60wt% dimethylacetamide, slowly heated to 60-80°C at a heating rate of 2-5°C per minute, stirred for 60-120 minutes to fully dissolve the polyurethane, add 0.01 wt % additive and fully stirred to obtain an antibacterial polyurethane electrospinning solution.

[0046] Next, the antibacterial polyurethane electrospinning solution was electrospun at a spinning speed of 12 ml / h and a voltage of 15 kV.

[0047] Finally, the obtained electrospinning fibers are dried at a temperature of 60° C. for 0.1-4 hours to remove the residual organic solvent to prepare antibacterial nanofibers.

Embodiment 3

[0049] First, an antimicrobial polymer resin solution is prepared.

[0050] Taking mass as the unit, dissolve 10wt% photosensitive molecule (model YG-03, the manufacturer is Qingdao Sunshine Biomedical Technology Co., Ltd.) into 10wt% formic acid (mass fraction ≥88%) solution, and the average molecular weight is 50,000 of 6wt% polymer resin was dissolved into 60wt% dimethylacetamide, slowly heated to 60-80°C at a heating rate of 2-5°C per minute, stirred for 60-120 minutes to fully dissolve the polyurethane, add 0.01 wt % additive and fully stirred to obtain an antibacterial polyurethane electrospinning solution.

[0051] Next, the antibacterial polyurethane electrospinning solution was electrospun at a spinning speed of 12 ml / h and a voltage of 15 kV.

[0052] Finally, the obtained electrospinning fibers are dried at a temperature of 60° C. for 0.1-4 hours to remove the residual organic solvent to prepare antibacterial nanofibers.

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Abstract

The invention discloses antibacterial nanofibers or master batches and a preparation method thereof, including components of an antibacterial polymer resin solution and the preparation method of the antibacterial nanofibers or master batches. The antibacterial nanofibers or master batches are characterized by being formed through electrostatic spinning, melt-blowing, fibrillation and two-component compound methods on antibacterial polymer resin solution. Photosensitive molecules in the antibacterial nanofibers or the antibacterial master batches are antibacterial, do not generate a dissolution phenomenon, and are high in efficiency, wide in spectrum and antibacterial; the high temperature resistance of an organic antibacterial agent material is effectively provided; and the application range of an antibacterial agent is further expanded.

Description

technical field [0001] The invention belongs to the field of textiles, and specifically relates to an antibacterial and mildew-proof antibacterial nanofiber or an antibacterial master batch and a preparation method thereof. Background technique [0002] Traditional nanofibers have a wide range of applications in air filtration, water treatment, catalysis, medicine and other fields due to their small fiber diameter, small pore size, high porosity, and large specific surface area. However, adding various small-molecule nanoparticles into the spinning solution not only increases the difficulty of the spinning process, but also greatly reduces the active point of the functional material, which greatly increases the cost. CN201510737628 discloses a method for preparing an antibacterial nanofiber membrane. The surface-modified porous nanofibers are used to form a shell-core structure membrane, and at the same time, some other nanoparticles, such as metallic silver, copper, zinc, m...

Claims

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Application Information

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IPC IPC(8): D01F1/10D01F8/16D01F8/12C08L75/04C08L77/04D01D5/00
CPCD01F1/103C08L75/04D01D5/003D01D5/0069D01D5/0092D01F8/12D01F8/16C08L77/04
Inventor 刘观峰王伟杰林帆
Owner SUNDYNAMIC TECH
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