Method for preparing nano-selenium-containing amino acid foliar fertilizer by regulation of radix platycodonis
The technology of Platycodon grandiflorum polysaccharide and nano-selenium, which is applied in the field of fertilizers, can solve the problems of high production cost, low biological activity and safety of nano-selenium and amino acids, and achieves improved use value and economic benefit, efficient utilization, improved yield and high efficiency. The effect of decolorization rate
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Embodiment 1
[0036] A method for regulating and preparing amino acid foliar fertilizer containing nano-selenium by platycodon polysaccharide, comprising the following steps:
[0037] (1) Preparation of nano-selenium solution
[0038] Mix selenous acid and bellflower polysaccharide solution, add water and stir evenly; add ascorbic acid solution, shake and mix well, so that the molar ratio of selenous acid and ascorbic acid in the reaction system is 1:3, and the concentration of selenous acid is 0.01mmol / L, The concentration of ascorbic acid is 0.03mmol / L, the mass fraction of Campanulaceae polysaccharide is 0.02%, the reaction mixture is placed in a water bath at a temperature of 80°C for 6 hours, the solution turns red, and a solution containing red nano-selenium is obtained;
[0039] (2) Preparation of amino acid solution
[0040] A. Preparation of soybean meal compound amino acid stock solution
[0041]Dry the soybean meal to remove impurities, pass through a 40-mesh sieve, add a 5mol / ...
Embodiment 2
[0049] A method for regulating and preparing amino acid foliar fertilizer containing nano-selenium by platycodon polysaccharide, comprising the following steps:
[0050] (1) Preparation of nano-selenium solution
[0051] Mix selenous acid and bellflower polysaccharide solution, add water and stir evenly; add ascorbic acid solution, shake and mix well, so that the molar ratio of selenous acid and ascorbic acid in the reaction system is 1:5, and the concentration of selenous acid is 0.01mmol / L, The concentration of ascorbic acid is 0.05mmol / L, the mass fraction of Platycodon grandiflorum is 0.02%, the reaction mixture is placed in a water bath at 60°C for 4 hours, the solution turns red, and a solution containing red nano-selenium is obtained;
[0052] (2) Preparation of amino acid solution
[0053] A. Preparation of soybean meal compound amino acid stock solution
[0054] Dry the soybean meal to remove impurities, pass through a 40-mesh sieve, and add a 3.1mol / L sulfuric acid...
Embodiment 3
[0062] A method for regulating and preparing amino acid foliar fertilizer containing nano-selenium by platycodon polysaccharide, comprising the following steps:
[0063] (1) Preparation of nano-selenium solution
[0064] Mix selenous acid and bellflower polysaccharide solution, add water and stir evenly; add ascorbic acid solution, shake and mix well, so that the molar ratio of selenous acid and ascorbic acid in the reaction system is 1:8, and the concentration of selenous acid is 0.01mmol / L, The concentration of ascorbic acid is 0.08mmol / L, the mass fraction of Campanulaceae polysaccharide is 0.02%, the reaction mixture is placed in a water bath at a temperature of 40°C for 2 hours, the solution turns red, and a solution containing red nano-selenium is obtained;
[0065] (2) Preparation of amino acid solution
[0066] A. Preparation of soybean meal compound amino acid stock solution
[0067] Dry the soybean meal to remove impurities, pass through a 40-mesh sieve, add 7mol / L...
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