Akebia trifoliate pectin beverage and preparation method thereof
A technology of cloverleaf and pectin, which is applied in the field of beverages, can solve the problems of difficult filtration of extracts, easily corroded equipment, unfavorable environmental protection, etc., and achieves the effects of mild action, convenient operation and fast hydrolysis.
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Embodiment 1
[0038] 1. Preparation of nanoscale carbon-based solid acid The preparation steps are as follows:
[0039] a), dissolving the six-carbon sugar in water, stirring at room temperature for 0.1-5h to form a 2mol / L aqueous solution; the six-carbon sugar is glucose;
[0040] b) Add mineral acid to the solution obtained in step a), and stir for 2-3 hours; the mineral acid is nitric acid; wherein the molar ratio of mineral acid to hexose is 3:1;
[0041] c), heat-treating the sample obtained in step b) at 90-120°C for 6-8h;
[0042] d), heat-treated samples were heat-treated at 600-650° C. for 10-12 h under nitrogen atmosphere to obtain nanoscale carbon-based solid acid.
[0043] Two, prepare Akebia trifoliate pectin extract:
[0044] 1) The peel of Akebia trifoliata washed with deionized water is dried, and then dried under reduced pressure at 40°C and a pressure of P=-0.07MPa to constant weight;
[0045]2) Crumble 10kg of dried Akebia pericarp into chunks below 0.2cm, and then pla...
Embodiment 2
[0057] The preparation method of nanoscale carbon-based solid acid is the same as in Example 1.
[0058] Except step 5) before adding ethanol, the extract was chelated with chelating agent calcium citrate and then filtered, and the filtrate was slowly dropped into ethanol to precipitate the pectin extract, and filtered and dried to obtain the rear end extract of Akebia trifoliata different from Example 1 Besides, the extraction method of the other Akebia trifoliate pectin extracts is exactly the same as in Example 1. The back-end extract of Akebia clover, namely Akebia clover pectin, is detected and calculated with reference to the teaching in "Anhui Agricultural Science" 2007, 35 (16): 4757-4759, and finally the back-end extract of Akebia clover of the present invention is Akebia clover The extraction rate of pectin is 16.2%.
[0059] To prepare akeba pectin drink:
[0060] 1) Weigh 6 parts by weight of Akebia trifoliate pectin extract and add it to 102 parts by weight of d...
Embodiment 3
[0064] The preparation method of nanoscale carbon-based solid acid is the same as in Example 1.
[0065] Except step 5) before adding ethanol, the extract was chelated with chelating agent calcium citrate and then filtered, and the filtrate was slowly dropped into ethanol to precipitate the pectin extract, and filtered and dried to obtain the rear end extract of Akebia trifoliata different from Example 1 Besides, the extraction method of the other Akebia trifoliate pectin extracts is exactly the same as in Example 1.
[0066] To prepare akeba pectin drink:
[0067] 1) Weigh 5 parts by weight of Akebia trifoliate pectin extract and add it to 100 parts by weight of deionized water, and cut it in a high-speed shearing machine at 0-5°C for 20-30 minutes;
[0068] 2) Add 0.2 parts by weight of calcium alginate, 0.2 parts by weight of riboflavin tetrabutyrate, and 0.2 parts by weight of D-(+)-N-(2,4-dihydroxy-3,3-dimethylbutyryl) -Calcium β-alanine and 0.3 parts by weight of calci...
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