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Preparation and application method of a storable high modulus natural asphalt binder

A technology of natural asphalt and cementitious materials, applied in building thermal insulation materials, building components, buildings, etc., can solve problems such as inability to apply, long-term storage application of products not mentioned, poor quality stability, etc.

Active Publication Date: 2018-04-06
西咸新区众力沥青有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The wet or dry process not only increases the construction process, but also has poor product quality stability and difficult quality control.
[0005] Chinese patents "A High Modulus Asphalt Based on Natural Asphalt Modification and Its Preparation Method and Application" 201410536546.9, "A High Modulus Asphalt and Its Preparation Method" 201410063471.7 both use natural asphalt as a modifier, which belongs to the wet process The use of natural asphalt does not produce a finished cementitious material, and it does not mention whether the product can be stored for a long time.
And the fatigue life of the mixture did not adopt the standard of more than 1 million times required by the French high modulus asphalt mixture
The Chinese patent "An energy-saving and environment-friendly asphalt and its preparation process" also mentions the way of using natural asphalt, various polymers and road petroleum asphalt to configure asphalt, and according to its implementation cases, the high-temperature rutting indicators are all less than 5000 times / mm , cannot be used in HMAC, and does not mention the storage stability of the product

Method used

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  • Preparation and application method of a storable high modulus natural asphalt binder
  • Preparation and application method of a storable high modulus natural asphalt binder
  • Preparation and application method of a storable high modulus natural asphalt binder

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] After heating 70#A grade road petroleum asphalt to 180°C, slowly add natural asphalt particles crushed to 300 mesh, wherein the mass ratio of natural asphalt to 70#A road petroleum asphalt is 70:30. And the natural asphalt is Trinidad Lake asphalt in South America, the asphaltene content is greater than 30%, the water content is lower than 2% after drying, the mixture is stirred and the temperature is raised to 185 ° C, and then it is ground in a ball mill for 2 hours to make the natural asphalt The average particle size of trichlorethylene insoluble particles in asphalt is 5000-10000 mesh and below to obtain a natural asphalt mother liquor; the natural asphalt mother liquor is mixed with Zhenhai 90A grade road petroleum asphalt heated to 160°C in a ratio of 60:40, and then Add 0.5% silane coupling agent and stir evenly, add 3% 1301 SBS modifier, after being sheared and dispersed by a shearing machine, add 0.7% sulfur, after 3 hours of development, add 0.1% sasobit and s...

Embodiment 2

[0041] After heating 110#A grade road petroleum asphalt to 180°C, slowly add natural asphalt particles crushed to 300 mesh, wherein the mass ratio of natural asphalt to 110#A road petroleum asphalt is 60:40. And the natural asphalt is rock asphalt, the asphaltene content is greater than 30%, and the moisture content is lower than 2% after drying treatment. After stirring and raising the temperature to 180°C, enter the ball mill for grinding for 2 hours to obtain the natural asphalt mother liquor; 90A grade asphalt heating After reaching 160°C, mix it with the above natural asphalt mother liquor at a ratio of 50:50, then add 0.3% silane coupling agent and stir evenly, add 2% 4303 SBS modifier, and shear and disperse with a shearing machine. Add 0.5% sulfur, develop for 3 hours, add 0.2% Evotherm and stir for half an hour to get the finished product. Among them, the addition ratio of silane coupling agent, SBS, sulfur and Evotherm is based on the mixture of natural asphalt mothe...

Embodiment 3

[0044] Take limestone or basalt aggregates and configure the mixture according to the following gradation. The aggregate was heated for more than 8 hours to reach a temperature of 200°C, the mixing temperature was set to 180°C, and the high modulus natural asphalt in Example 1 was heated to 180°C. Put aggregates other than mineral powder into the mixing pot, and add asphalt after 20 seconds of dry mixing. The amount of asphalt is 5.2%. After mixing for 60 seconds, pour in mineral powder and mix for 30 seconds. Table 11 shows the gradation of the mixture.

[0045]

[0046] According to the French mixture detection index and the domestic Marshall test method, the performance of the mixture is verified respectively: Table 12 shows the mixture index results tested according to the French standard.

[0047]

[0048] According to the domestic Marshall test method, the various performance tests of the mixture are as follows: Table 13 shows the test results of the EME2 0 / 14 mixt...

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Abstract

The invention relates to a preparation and application method of a storable high-modulus natural asphalt cementing material. The method comprises the following steps: mixing natural asphalt which is crushed into 300 meshes with soft asphalt which is heated to be 190 to 200 DEG C according to a ratio of 1: 3 to 5:1 at room temperature, enabling an obtained mixture to enter a grinding machine, grinding for 1 to 2h to obtain a natural asphalt mother solution with an average particle size of trichloro ethylene insoluble substances in the natural asphalt less than or equal to 5000 to 10000 meshes; mixing the mother solution and road petroleum asphalt with the temperature of 130 to 150 DEG C according to a weight ratio of 30: 70 to 70:30 to obtain a mixture A, adding a coupling agent accounting for 0.1 to 2 percent of the weight of the mixture A, uniformly stirring, adding a polymer modifier accounting for 0 to 10 percent of the weight of the mixture A, shearing, dispersing, then adding the cross-linking agent, developing for 2 to 5 h at the temperature lower than 180 to 190 DEG C, adding a viscosity reducer, and stirring for half an hour to obtain the storable high-modulus natural asphalt cementing material, wherein the cross-linking agent and the viscosity reducer respectively account for 0 to 0.3 percent and 0.1 to 1 percent of the weight of the mixture A. The high-modulus asphalt mixture cementing material is firstly prepared in a form of a finished product material, the product can be stored and transported for a long time without being separated, and the prepared mixture has excellent characteristics of high-modulus asphalt mixture and excellent low-temperature performance.

Description

technical field [0001] This patent belongs to the field of road building materials and specifically relates to a preparation and application method of a storable asphalt binder specially used for high modulus asphalt mixture. Background technique [0002] High Modulus Asphalt Mixture (HMAC: High Modules Asphalt Concrete for short) originated in France. Due to its high overall modulus and good fatigue resistance, it was introduced and absorbed by Britain, South Africa, the United States, Finland, China and other countries. It is used to solve the problems of road surface rutting under the condition of sudden increase in traffic volume and heavy load. According to the definition of French asphalt mixture design specification (NFP98-140), when the dynamic modulus (15°C, 10Hz) of asphalt mixture is greater than 14000Mpa, it is called "high modulus asphalt mixture". After HMAC was introduced into China, it was mainly used in the middle and lower layers of asphalt pavement. Its a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L95/00C08L53/02C08L9/06C08L21/00C08K13/02C08K5/54C08K5/10C08K5/521C08K3/06C08K5/36C04B26/26
CPCC04B26/26C08L95/00C08L2205/025C08L2205/035C08L53/02C08L9/06C08L21/00C08K13/02C08K5/54C08K5/10C08K5/521C08K3/06C08K5/36C04B24/42C04B24/24C04B2103/0068C04B24/34C04B14/28C04B14/04C04B2103/40C04B24/40C04B24/003
Inventor 曾赟张俊搏张玲张彬韩筱东张晓宏
Owner 西咸新区众力沥青有限公司