Method for preparing fireproof high-temperature resistant plate

A high-temperature-resistant and plate-based technology, which is applied in the field of preparation of fire-resistant and high-temperature-resistant plates, can solve the problems of large impact on fireproof performance, poor high-temperature resistance, property loss, etc., and achieve improved stability, flame-retardant efficiency, and water resistance. , the effect of water solubility reduction

Inactive Publication Date: 2017-09-26
安徽三义和能源科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] There are many uses of fireproof panels, which can be used in the construction of building exterior walls, interior walls, temporary houses, etc. The fireproof performance has a great influence on the performance of the panels. If the panels have poor fireproof performance, there will be greater safety hazards
If exposed to an open flame, causing the plate to burn rapidly, it will cause serious property damage
In addition, if the high temperature resistance of the board is poor, under high temperature conditions, the board will be deformed after being heated for a long time, which will pose a great test to the stability of the building. Therefore, we need to find a good fire resistance and Plates with high temperature resistance

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] A kind of preparation method of fireproof and high temperature resistant board proposed by the present invention comprises the following steps:

[0015] S1. Mix melamine, formaldehyde, and water evenly, adjust the pH value of the system to 9-9.7 with sodium hydroxide, heat up and stir, add microcrystalline cellulose, cocamidopropyl betaine, and adjust the pH value of the system to 5-9.7 with hydrochloric acid. 5.4, ​​add castor oil and polyethylene glycol, stir, and cool to obtain pretreated microcrystalline cellulose;

[0016] S2. Mix phenolic epoxy resin, polyamide resin, microcapsule red phosphorus and ammonium polyphosphate evenly, add water and tartaric acid and stir evenly, then add pretreated microcrystalline cellulose, calcium sulfate, fumed silica, talcum powder, The magnesium hydroxide is mixed and stirred evenly, put into a mold for pressing, and cooled to room temperature to obtain a fireproof and high temperature resistant plate.

Embodiment 2

[0018] A kind of preparation method of fireproof and high temperature resistant board proposed by the present invention comprises the following steps:

[0019] S1. Mix 10 parts of melamine, 12 parts of formaldehyde, and 120 parts of water in parts by weight, adjust the pH of the system to 9-9.7 with sodium hydroxide, heat up to 90°C and stir for 20 minutes, add 30 parts of microcrystalline cellulose, 1 part of For cocamidopropyl betaine, use hydrochloric acid to adjust the pH value of the system to 5-5.4, add 35 parts of castor oil and 8 parts of polyethylene glycol and stir for 50 minutes, the stirring temperature is 75 ° C, the stirring speed is 1000 r / min, and the pre- processing microcrystalline cellulose;

[0020] S2. Mix 50 parts of novolak epoxy resin, 30 parts of polyamide resin, 40 parts of microcapsule red phosphorus, and 8 parts of ammonium polyphosphate in parts by weight, add 20 parts of water and 7 parts of tartaric acid and stir evenly, and then add 20 parts of ...

Embodiment 3

[0022] A kind of preparation method of fireproof and high temperature resistant board proposed by the present invention comprises the following steps:

[0023] S1. Mix 16 parts of melamine, 6 parts of formaldehyde, and 160 parts of water in parts by weight, adjust the pH of the system to 9-9.7 with sodium hydroxide, heat up to 85°C and stir for 30 minutes, add 20 parts of microcrystalline cellulose, 2 parts of For cocamidopropyl betaine, use hydrochloric acid to adjust the pH value of the system to 5-5.4, add 25 parts of castor oil and 16 parts of polyethylene glycol and stir for 30 minutes, the stirring temperature is 85 ° C, the stirring speed is 800 r / min, and the pre- processing microcrystalline cellulose;

[0024] S2. Mix 70 parts of novolac epoxy resin, 20 parts of polyamide resin, 60 parts of microcapsule red phosphorus, and 6 parts of ammonium polyphosphate in parts by weight, add 40 parts of water and 3 parts of tartaric acid and stir evenly, and then add 30 parts of ...

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PUM

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Abstract

The invention discloses a method for preparing a fireproof high-temperature resistant plate. The method comprises the following steps: uniformly mixing melamine, formaldehyde and water, adjusting the pH value of the system to be 9-9.7 by using sodium hydroxide, performing heating stirring, adding microcrystalline cellulose and cocamidopropyl betaine, adjusting the pH value of the system to 5-5.4 by using hydrochloric acid, adding castor oil and polyethylene glycol, stirring, and cooling so as to obtain pretreated microcrystalline cellulose; uniformly mixing phenolic aldehyde epoxy resin, polyamide resin, microencapsulated red phosphorus and ammonium polyphosphate, adding water and tartaric acid, uniformly stirring, further adding the pretreated microcrystalline cellulose, calcium sulfate, fumed silica, talcum powder and magnesium hydrate, uniformly mixing and stirring, performing pressing molding in a mold, and cooling to the room temperature, thereby obtaining the fireproof high-temperature resistant plate. The fireproof high-temperature resistant plate is good in compatibility, excellent in fire and high temperature resistance, excellent in water resistance and free of moisture absorption phenomenon.

Description

technical field [0001] The invention relates to the technical field of boards, in particular to a method for preparing fireproof and high temperature resistant boards. Background technique [0002] There are many uses of fireproof panels, which can be used in the construction of building exterior walls, interior walls, temporary houses, etc. The fire performance has a great influence on the performance of the panels. If the panels have poor fire performance, there will be greater safety hazards . If it encounters an open flame, the plate will burn rapidly, which will cause serious property loss. In addition, if the high temperature resistance of the board is poor, under high temperature conditions, the board will be deformed after being heated for a long time, which will pose a great test to the stability of the building. Therefore, we need to find a good fire resistance and Plates with high temperature resistance. Contents of the invention [0003] Based on the technic...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L63/00C08L77/00C08L61/06C08L1/04C08L91/00C08L71/02C08K13/06C08K9/10C08K3/02C08K3/32C08K3/30C08K3/36C08K3/34C08K3/22C08K5/092B29D7/01
CPCC08L63/00B29D7/01C08K2003/026C08K2003/2224C08K2003/3045C08K2003/323C08L2201/02C08L2201/08C08L2205/035C08L77/00C08L61/06C08L1/04C08L91/00C08L71/02C08K13/06C08K9/10C08K3/02C08K3/32C08K3/30C08K3/36C08K3/34C08K3/22C08K5/092
Inventor 冯益生
Owner 安徽三义和能源科技有限公司
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